<2S-(2α,3aα,4aβ,5α,8α,8aβ)>-Octahydro-2-<2-(benzyloxy)ethyl>-3a-<4-(benzyloxy)butyl>-5,10,10-trimethyl-5,8-methano-2H-isoxazolo<3,2-b>benzoxazole

Base Information

Chemical Name:<2S-(2α,3aα,4aβ,5α,8α,8aβ)>-Octahydro-2-<2-(benzyloxy)ethyl>-3a-<4-(benzyloxy)butyl>-5,10,10-trimethyl-5,8-methano-2H-isoxazolo<3,2-b>benzoxazole
CAS No.:162284-05-1
Molecular Formula:C₃₃H₄₅NO₄
Molecular Weight:519.725
Hs Code.:

Synonyms:<2S-(2α,3aα,4aβ,5α,8α,8aβ)>-Octahydro-2-<2-(benzyloxy)ethyl>-3a-<4-(benzyloxy)butyl>-5,10,10-trimethyl-5,8-methano-2H-isoxazolo<3,2-b>benzoxazole

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Chemical Property of <2S-(2α,3aα,4aβ,5α,8α,8aβ)>-Octahydro-2-<2-(benzyloxy)ethyl>-3a-<4-(benzyloxy)butyl>-5,10,10-trimethyl-5,8-methano-2H-isoxazolo<3,2-b>benzoxazole

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Technology Process of <2S-(2α,3aα,4aβ,5α,8α,8aβ)>-Octahydro-2-<2-(benzyloxy)ethyl>-3a-<4-(benzyloxy)butyl>-5,10,10-trimethyl-5,8-methano-2H-isoxazolo<3,2-b>benzoxazole

There total 6 articles about <2S-(2α,3aα,4aβ,5α,8α,8aβ)>-Octahydro-2-<2-(benzyloxy)ethyl>-3a-<4-(benzyloxy)butyl>-5,10,10-trimethyl-5,8-methano-2H-isoxazolo<3,2-b>benzoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60789-54-0
4-bromobutyl benzyl ether

: 162284-05-1
<2S-(2α,3aα,4aβ,5α,8α,8aβ)>-Octahydro-2-<2-(benzyloxy)ethyl>-3a-<4-(benzyloxy)butyl>-5,10,10-trimethyl-5,8-methano-2H-isoxazolo<3,2-b>benzoxazole

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / t-BuOK, Aliquat 336 / 4 h / 25 °C

2: toluene / 60 h / 80 °C

With potassium tert-butylate; Aliquat 336; In toluene;
DOI:10.1021/jo00111a033

Reference yield:

: 91477-32-6
5-(Benzyloxy)pentane nitrile

: 162284-05-1
<2S-(2α,3aα,4aβ,5α,8α,8aβ)>-Octahydro-2-<2-(benzyloxy)ethyl>-3a-<4-(benzyloxy)butyl>-5,10,10-trimethyl-5,8-methano-2H-isoxazolo<3,2-b>benzoxazole

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / HCl / diethyl ether / 48 h / 0 °C

2: 75 percent / hexane / 48 h

3: 4 Angstroem molecular sieves / CH₂Cl₂ / 2 h / 40 °C

4: toluene / 60 h / 80 °C

With hydrogenchloride; 4 A molecular sieve; In diethyl ether; hexane; dichloromethane; toluene;
DOI:10.1021/jo00111a033

Reference yield:

: (+)-3-(hydroxylamino)isoborneol hydrochloride

: 162284-05-1
<2S-(2α,3aα,4aβ,5α,8α,8aβ)>-Octahydro-2-<2-(benzyloxy)ethyl>-3a-<4-(benzyloxy)butyl>-5,10,10-trimethyl-5,8-methano-2H-isoxazolo<3,2-b>benzoxazole

Guidance literature:: Multi-step reaction with 2 steps

1: 4 Angstroem molecular sieves / CH₂Cl₂ / 2 h / 40 °C

2: toluene / 60 h / 80 °C

With 4 A molecular sieve; In dichloromethane; toluene;
DOI:10.1021/jo00111a033