Technology Process of C16H25NO2
There total 6 articles about C16H25NO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
(R)-2-Methyl-4-oxo-butyric acid tert-butyl ester; benzylamine;
With
magnesium sulfate;
In
dichloromethane;
at 20 ℃;
for 15h;
With
sodium tris(acetoxy)borohydride;
In
dichloromethane;
at 20 ℃;
for 3h;
DOI:10.1021/ol400207t
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 10 wt% Pd(OH)2 on carbon; hydrogen / ethyl acetate / 16 h / 20 °C
2.1: C50H73O4P / dichloromethane / 240 h / 5 °C / Inert atmosphere
3.1: pyridinium chlorochromate / dichloromethane / 6 h
4.1: magnesium sulfate / dichloromethane / 15 h / 20 °C
4.2: 3 h / 20 °C
With
10 wt% Pd(OH)2 on carbon; C50H73O4P; hydrogen; magnesium sulfate; pyridinium chlorochromate;
In
dichloromethane; ethyl acetate;
DOI:10.1021/ol400207t
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: pyridinium chlorochromate / dichloromethane / 6 h
2.1: magnesium sulfate / dichloromethane / 15 h / 20 °C
2.2: 3 h / 20 °C
With
magnesium sulfate; pyridinium chlorochromate;
In
dichloromethane;
DOI:10.1021/ol400207t