Cyclohexanemethanol, 1-ethenyl-2-hydroxy-, (1R,2S)-rel- (9CI)

Base Information

• Chemical Name: Cyclohexanemethanol, 1-ethenyl-2-hydroxy-, (1R,2S)-rel- (9CI)
• CAS No.: 745810-78-0
• Molecular Formula: C₉H₁₆O₂
• Molecular Weight: 156.225
• Mol file: 745810-78-0.mol

Synonyms:Cyclohexanemethanol, 1-ethenyl-2-hydroxy-, (1R,2S)-rel- (9CI)

Chemical Property of Cyclohexanemethanol, 1-ethenyl-2-hydroxy-, (1R,2S)-rel- (9CI)

Chemical Property:

• PSA: 40.46000
• LogP: 1.08600

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of Cyclohexanemethanol, 1-ethenyl-2-hydroxy-, (1R,2S)-rel- (9CI)

There total 2 articles about Cyclohexanemethanol, 1-ethenyl-2-hydroxy-, (1R,2S)-rel- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-methylene-7-octen-1-al (71304-42-2) → (1R,2R)-2-Hydroxymethyl-2-vinyl-cyclohexanol (745810-78-0) + (1S,2R)-2-Hydroxymethyl-2-vinyl-cyclohexanol (745810-78-0)

Guidance literature:

6-methylene-7-octen-1-al; With 2,2'-bis(1,3,2-benzodioxaborole); ethylenebis(triphenylphosphine)platinum⁽⁰⁾; In tetrahydrofuran; at 60 ℃; for 24h;

With sodium hydroxide; dihydrogen peroxide; In tetrahydrofuran; at 20 ℃; for 3h; Title compound not separated from byproducts;

DOI:10.1055/s-2004-822379

Reference yield:

6-methylene-7-octen-1-al (71304-42-2) → (1R,2R)-2-Hydroxymethyl-2-vinyl-cyclohexanol (745810-78-0) + (1S,2R)-2-Hydroxymethyl-2-vinyl-cyclohexanol (745810-78-0)

Guidance literature:

6-methylene-7-octen-1-al; With 2,2'-bis(1,3,2-benzodioxaborole); ethylenebis(triphenylphosphine)platinum⁽⁰⁾; In tetrahydrofuran; at 60 ℃; for 24h;

With sodium hydroxide; dihydrogen peroxide; In tetrahydrofuran; at 20 ℃; for 3h; Title compound not separated from byproducts;

DOI:10.1055/s-2004-822379

upstream raw materials:

6-methylene-7-octen-1-al

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