3-<2-O-(methoxymethyl)-2-hydroxyphenyl>-3,3-dimethyl-1-propylphthalimide

Base Information

Chemical Name:3-<2-O-(methoxymethyl)-2-hydroxyphenyl>-3,3-dimethyl-1-propylphthalimide
CAS No.:121374-69-4
Molecular Formula:C₂₁H₂₃NO₄
Molecular Weight:353.418
Hs Code.:

Synonyms:3-<2-O-(methoxymethyl)-2-hydroxyphenyl>-3,3-dimethyl-1-propylphthalimide

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Chemical Property of 3-<2-O-(methoxymethyl)-2-hydroxyphenyl>-3,3-dimethyl-1-propylphthalimide

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Technology Process of 3-<2-O-(methoxymethyl)-2-hydroxyphenyl>-3,3-dimethyl-1-propylphthalimide

There total 3 articles about 3-<2-O-(methoxymethyl)-2-hydroxyphenyl>-3,3-dimethyl-1-propylphthalimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1074-82-4
potassium phtalimide

: 121374-68-3
3-<2-O-(methoxymethyl)-2-hydroxyphenyl>-3,3'-dimethyl-1-propyl tosylate

: 121374-69-4
3-<2-O-(methoxymethyl)-2-hydroxyphenyl>-3,3-dimethyl-1-propylphthalimide

Guidance literature:: In N,N-dimethyl-formamide; at 60 ℃; for 18h;
DOI:10.1021/jo00275a034

Reference yield:

: 40614-20-8
3-(2'-Hydroxyphenyl)-3,3-dimethylpropanol

: 121374-69-4
3-<2-O-(methoxymethyl)-2-hydroxyphenyl>-3,3-dimethyl-1-propylphthalimide

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / sodium hydride / tetrahydrofuran / 6 h / 0 - 20 °C

2: 100 percent / pyridine / 18 h / 4 °C

3: 90 percent / dimethylformamide / 18 h / 60 °C

With pyridine; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo00275a034

Reference yield:

: 121374-67-2
3-<2-O-(methoxymethyl)-2-hydroxyphenyl>-3,3-dimethyl-1-propanol

: 121374-69-4
3-<2-O-(methoxymethyl)-2-hydroxyphenyl>-3,3-dimethyl-1-propylphthalimide

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / pyridine / 18 h / 4 °C

2: 90 percent / dimethylformamide / 18 h / 60 °C

With pyridine; In N,N-dimethyl-formamide;
DOI:10.1021/jo00275a034