p-Methoxybenzyl 2α-methyl-2β-<(R)-acetoxymethoxymethyl>-6β-(phenoxyacetamido)penam-3α-carboxylate

Base Information

Chemical Name:p-Methoxybenzyl 2α-methyl-2β-<(R)-acetoxymethoxymethyl>-6β-(phenoxyacetamido)penam-3α-carboxylate
CAS No.:70942-89-1
Molecular Formula:C₂₇H₃₀N₂O₉S
Molecular Weight:558.609
Hs Code.:

Synonyms:p-Methoxybenzyl 2α-methyl-2β-<(R)-acetoxymethoxymethyl>-6β-(phenoxyacetamido)penam-3α-carboxylate

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Chemical Property of p-Methoxybenzyl 2α-methyl-2β-<(R)-acetoxymethoxymethyl>-6β-(phenoxyacetamido)penam-3α-carboxylate

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Technology Process of p-Methoxybenzyl 2α-methyl-2β-<(R)-acetoxymethoxymethyl>-6β-(phenoxyacetamido)penam-3α-carboxylate

There total 1 articles about p-Methoxybenzyl 2α-methyl-2β-<(R)-acetoxymethoxymethyl>-6β-(phenoxyacetamido)penam-3α-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 58747-45-8
p-Methoxybenzyl 2α-methoxy-3α-bromo-3β-methyl-7-(phenoxyacetamido)cepham-4-carboxylate

: 70942-89-1
p-Methoxybenzyl 2α-methyl-2β-<(R)-acetoxymethoxymethyl>-6β-(phenoxyacetamido)penam-3α-carboxylate

: 73156-59-9
p-Methoxybenzyl 2α-methyl-2β-<(S)-acetoxymethoxymethyl>-6β-(phenoxyacetamido)penam-3α-carboxylate

Guidance literature:: With silver(I) acetate; In acetic acid; at 100 ℃; for 0.25h;
DOI:10.1021/jo01301a014

Reference yield:

: 70942-89-1
p-Methoxybenzyl 2α-methyl-2β-<(R)-acetoxymethoxymethyl>-6β-(phenoxyacetamido)penam-3α-carboxylate

: 73156-60-2
2α-Methyl-2β-< (R)-acetoxymethoxymethyl >-6β-(phenoxyacetamido)penam-3α-carboxylic acid

Guidance literature:: With hydrogen; Lindlar's catalyst; In 1,4-dioxane; water; Ambient temperature;
DOI:10.1021/jo01301a014

Reference yield:

: 70942-89-1
p-Methoxybenzyl 2α-methyl-2β-<(R)-acetoxymethoxymethyl>-6β-(phenoxyacetamido)penam-3α-carboxylate

: 73156-68-0
(5S,6R,7R)-3-[(2,4-Dinitro-phenyl)-hydrazonomethyl]-5,8-dioxo-7-(2-phenoxy-acetylamino)-5λ⁴-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid 4-methoxy-benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 mg / m-Cl-C₆H₄-CO₃H / CH₂Cl₂ / 2 h / 0 °C

2: 120 mg / benzene / 1 h / Heating

3: 12 mg / H₂SO₄ / aq. ethanol / 1 h

With 3-chloro-benzenecarboperoxoic acid; sulfuric acid; In ethanol; dichloromethane; benzene;
DOI:10.1021/jo01301a014