3-(N-(4-(benzyloxy)benzyl)-4-methylphenylsulfonamido)-N-methoxy-N-methylpropanamide

Base Information

Chemical Name:3-(N-(4-(benzyloxy)benzyl)-4-methylphenylsulfonamido)-N-methoxy-N-methylpropanamide
CAS No.:1579268-57-7
Molecular Formula:C₂₆H₃₀N₂O₅S
Molecular Weight:482.601
Hs Code.:

Synonyms:3-(N-(4-(benzyloxy)benzyl)-4-methylphenylsulfonamido)-N-methoxy-N-methylpropanamide

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Chemical Property of 3-(N-(4-(benzyloxy)benzyl)-4-methylphenylsulfonamido)-N-methoxy-N-methylpropanamide

Chemical Property:

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Technology Process of 3-(N-(4-(benzyloxy)benzyl)-4-methylphenylsulfonamido)-N-methoxy-N-methylpropanamide

There total 1 articles about 3-(N-(4-(benzyloxy)benzyl)-4-methylphenylsulfonamido)-N-methoxy-N-methylpropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 193635-17-5
N-methoxy-N-methyl-3-((4-methylphenyl)sulfonamido)propanamide

: 836-42-0
4-benzyloxybenzyl chloride

: 1579268-57-7
3-(N-(4-(benzyloxy)benzyl)-4-methylphenylsulfonamido)-N-methoxy-N-methylpropanamide

Guidance literature:: N-methoxy-N-methyl-3-((4-methylphenyl)sulfonamido)propanamide; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.5h;

4-benzyloxybenzyl chloride; With tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; mineral oil; at 0 - 60 ℃; for 2h;
DOI:10.1016/j.tet.2014.01.074

Reference yield:

: 1579268-57-7
3-(N-(4-(benzyloxy)benzyl)-4-methylphenylsulfonamido)-N-methoxy-N-methylpropanamide

: C₂₄H₂₅NO₄S

Guidance literature:: With diisobutylaluminium hydride; In hexane; dichloromethane; at -78 ℃; for 0.333333h;
DOI:10.1016/j.tet.2014.01.074

Reference yield:

: 1579268-57-7
3-(N-(4-(benzyloxy)benzyl)-4-methylphenylsulfonamido)-N-methoxy-N-methylpropanamide

: 1579268-61-3
N-(4-(benzyloxy)benzyl)-N-(3-hydroxy-3-(1-tosyl-1H-indol-2-yl)propyl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: diisobutylaluminium hydride / dichloromethane; hexane / 0.33 h / -78 °C

2.1: isopropylmagnesium chloride / tetrahydrofuran / 0.5 h / 0 °C

2.2: 0.67 h / 0 °C

With isopropylmagnesium chloride; diisobutylaluminium hydride; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1016/j.tet.2014.01.074