biphenyl-2-ylcarbamic acid 1-{2-[5-(4-hydroxybenzylamino)pentyl-carbamoyl]ethyl}piperidin-4-yl ester

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Chemical Name:biphenyl-2-ylcarbamic acid 1-{2-[5-(4-hydroxybenzylamino)pentyl-carbamoyl]ethyl}piperidin-4-yl ester
CAS No.:864782-17-2
Molecular Formula:C₃₃H₄₂N₄O₄
Molecular Weight:558.721
Hs Code.:

Synonyms:biphenyl-2-ylcarbamic acid 1-{2-[5-(4-hydroxybenzylamino)pentyl-carbamoyl]ethyl}piperidin-4-yl ester

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Chemical Property of biphenyl-2-ylcarbamic acid 1-{2-[5-(4-hydroxybenzylamino)pentyl-carbamoyl]ethyl}piperidin-4-yl ester

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Technology Process of biphenyl-2-ylcarbamic acid 1-{2-[5-(4-hydroxybenzylamino)pentyl-carbamoyl]ethyl}piperidin-4-yl ester

There total 1 articles about biphenyl-2-ylcarbamic acid 1-{2-[5-(4-hydroxybenzylamino)pentyl-carbamoyl]ethyl}piperidin-4-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 909414-36-4
Biphenyl-2-ylcarbamic Acid 1-[2-(5-aminopentylcarbamoyl)ethyl]piperidin-4-yl Ester

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 864782-17-2
biphenyl-2-ylcarbamic acid 1-{2-[5-(4-hydroxybenzylamino)pentyl-carbamoyl]ethyl}piperidin-4-yl ester

Guidance literature:: Biphenyl-2-ylcarbamic Acid 1-[2-(5-aminopentylcarbamoyl)ethyl]piperidin-4-yl Ester; 4-hydroxy-benzaldehyde; In methanol; for 1h;

With sodium tris(acetoxy)borohydride; In methanol; at 20 ℃; for 2h;

With sodium hydroxide; In water; pH=13 - 14;

Reference yield:

: 864782-17-2
biphenyl-2-ylcarbamic acid 1-{2-[5-(4-hydroxybenzylamino)pentyl-carbamoyl]ethyl}piperidin-4-yl ester

: 76-05-1
trifluoroacetic acid

: 3-[(5-{3-[4-(biphenyl-2ylcarbamoyloxy)piperidin-1-yl]propionylamino}pentyl)(4-hydroxybenzyl)amino]propionic acid bis(trifluoroacetate)

Guidance literature:: 3-Bromopropionic acid; biphenyl-2-ylcarbamic acid 1-{2-[5-(4-hydroxybenzylamino)pentyl-carbamoyl]ethyl}piperidin-4-yl ester; With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 50 ℃;

trifluoroacetic acid;

Reference yield:

: 864782-17-2
biphenyl-2-ylcarbamic acid 1-{2-[5-(4-hydroxybenzylamino)pentyl-carbamoyl]ethyl}piperidin-4-yl ester

: 76-05-1
trifluoroacetic acid

: biphenyl-2-ylcarbamic acid 1-(2-{5-[(4-hydroxybenzyl)-(2-methylcarbamoylethyl)amino]pentylcarbamoyl}ethyl)piperidin-4-yl ester trifluoroacetate

Guidance literature:: 3-Bromopropionic acid; biphenyl-2-ylcarbamic acid 1-{2-[5-(4-hydroxybenzylamino)pentyl-carbamoyl]ethyl}piperidin-4-yl ester; With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 50 ℃;

methylamine; With HATU; In acetonitrile; at 20 ℃; for 2h;

trifluoroacetic acid;