N,N'-bis(p-methoxybenzyl)-1'-O-(trifluoroacetyl)-2',3'-O-isopropylidene-bicyclomycin

Base Information

Chemical Name:N,N'-bis(p-methoxybenzyl)-1'-O-(trifluoroacetyl)-2',3'-O-isopropylidene-bicyclomycin
CAS No.:92125-62-7
Molecular Formula:C₃₃H₃₇F₃N₂O₁₀
Molecular Weight:678.659
Hs Code.:

Synonyms:N,N'-bis(p-methoxybenzyl)-1'-O-(trifluoroacetyl)-2',3'-O-isopropylidene-bicyclomycin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-bis(p-methoxybenzyl)-1'-O-(trifluoroacetyl)-2',3'-O-isopropylidene-bicyclomycin

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Technology Process of N,N'-bis(p-methoxybenzyl)-1'-O-(trifluoroacetyl)-2',3'-O-isopropylidene-bicyclomycin

There total 19 articles about N,N'-bis(p-methoxybenzyl)-1'-O-(trifluoroacetyl)-2',3'-O-isopropylidene-bicyclomycin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 92098-17-4
N,N'-bis(p-methoxybenzyl)-2',3'-O-isopropylidene-bicyclomycin

: 407-25-0
trifluoroacetic anhydride

: 92125-62-7
N,N'-bis(p-methoxybenzyl)-1'-O-(trifluoroacetyl)-2',3'-O-isopropylidene-bicyclomycin

Guidance literature:: With dmap; In dichloromethane; for 0.416667h; Ambient temperature;
DOI:10.1021/ja00297a035

Reference yield:

: 81600-36-4
(+/-)-2,2,4-trimethyl-1,3-dioxolane-4-carboxaldehyde

: 92125-62-7
N,N'-bis(p-methoxybenzyl)-1'-O-(trifluoroacetyl)-2',3'-O-isopropylidene-bicyclomycin

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) THF, -98 deg C, 3 min; 2.) -98 deg C, 10 min, then --> room temp.

2: 95 percent / (dimethylamino)pyridine / CH₂Cl₂ / 0.42 h / Ambient temperature

With dmap; n-butyllithium; In dichloromethane;
DOI:10.1021/ja00297a035

Reference yield:

: 92098-15-2
8,10-bis(p-methoxybenzyl)-8,10-diaza-5-methylene-2-oxabicyclo<4.2.2>decane-7,9-dione

: 92125-62-7
N,N'-bis(p-methoxybenzyl)-1'-O-(trifluoroacetyl)-2',3'-O-isopropylidene-bicyclomycin

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) HMPA, n-butyllithium; 2.) O₂ / 1.) THF, -78 deg C, 7 min; 2.) THF, -78 deg C, 10 min, then --> room temp., 3 min

2: 1.) n-BuLi / 1.) THF, -98 deg C, 3 min; 2.) -98 deg C, 10 min, then --> room temp.

3: 95 percent / (dimethylamino)pyridine / CH₂Cl₂ / 0.42 h / Ambient temperature

With N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; n-butyllithium; oxygen; In dichloromethane;
DOI:10.1021/ja00297a035