N-[3-(3,7,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1⁽¹⁶⁾,13⁽¹⁷⁾,14-trien-7-yl)-propyl]-benzamide

Base Information

• Chemical Name: N-[3-(3,7,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1⁽¹⁶⁾,13⁽¹⁷⁾,14-trien-7-yl)-propyl]-benzamide
• CAS No.: 557083-65-5
• Molecular Formula: C₂₃H₃₃N₅O
• Molecular Weight: 395.548

Synonyms:N-[3-(3,7,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1⁽¹⁶⁾,13⁽¹⁷⁾,14-trien-7-yl)-propyl]-benzamide

Chemical Property of N-[3-(3,7,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1⁽¹⁶⁾,13⁽¹⁷⁾,14-trien-7-yl)-propyl]-benzamide

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Technology Process of N-[3-(3,7,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1⁽¹⁶⁾,13⁽¹⁷⁾,14-trien-7-yl)-propyl]-benzamide

There total 1 articles about N-[3-(3,7,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1⁽¹⁶⁾,13⁽¹⁷⁾,14-trien-7-yl)-propyl]-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

→ N-[3-(3,7,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1(16),13(17),14-trien-7-yl)-propyl]-benzamide (557083-65-5)

Guidance literature:

With sodium cyanide; In water;

DOI:10.1039/b211489e

Reference yield: 95.0%

copper(II) perchlorate hexahydrate + N-[3-(3,7,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1(16),13(17),14-trien-7-yl)-propyl]-benzamide (557083-65-5) → [Cu(C5H3N(CH2NHCH2CH2CH2)2NCH2CH2CH2NHCOC6H5)](2+)*2ClO4(1-)=[Cu(C5H3N(CH2NHCH2CH2CH2)2NCH2CH2CH2NHCOC6H5)](ClO4)2

Guidance literature:

In ethanol; a soln. of Cu-contg. compd. (1 equiv.) in ethanol was added to a soln. of a ligand (0.044 mmol) in the same solvent; the ppt. was collected and washed with cold ether; the ethanol filtrate was concd. and placed in the freezer (-10°C) for a few hours; theppt. was collected and washed with ether; the complex was dried overnig ht under vac.;

DOI:10.1039/b211489e

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