dibenzyl (2,2-dimethylhex-4-en-1-yl)aminomethylylidenebiscarbamate

Base Information

• Chemical Name: dibenzyl (2,2-dimethylhex-4-en-1-yl)aminomethylylidenebiscarbamate
• CAS No.: 1041482-38-5
• Molecular Formula: C₂₅H₃₁N₃O₄
• Molecular Weight: 437.539
• Mol file: 1041482-38-5.mol

Synonyms:dibenzyl (2,2-dimethylhex-4-en-1-yl)aminomethylylidenebiscarbamate

Chemical Property of dibenzyl (2,2-dimethylhex-4-en-1-yl)aminomethylylidenebiscarbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of dibenzyl (2,2-dimethylhex-4-en-1-yl)aminomethylylidenebiscarbamate

There total 1 articles about dibenzyl (2,2-dimethylhex-4-en-1-yl)aminomethylylidenebiscarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

N,N'-bis(benzyloxycarbonyl)-N''-trifluoromethane-sulfonylguanidine (207857-19-0) + 2,2-dimethyl-1-amino-5-hexene (141511-50-4) → dibenzyl (2,2-dimethylhex-4-en-1-yl)aminomethylylidenebiscarbamate (1041482-38-5)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 16h;

DOI:10.1039/b719479j

Reference yield: 88.0%

dibenzyl (2,2-dimethylhex-4-en-1-yl)aminomethylylidenebiscarbamate (1041482-38-5) → benzyl 3-(benzyloxycarbonylimino)-6,6-dimethylhexahydroimidazo[1,5-a]pyridine-2(1H)-carboxylate (1041482-44-3)

Guidance literature:

With palladium diacetate; potassium carbonate; copper dichloride; In N,N-dimethyl-formamide; at 20 ℃; for 14h;

DOI:10.1039/b719479j

upstream raw materials:

N,N'-bis(benzyloxycarbonyl)-N''-trifluoromethane-sulfonylguanidine

2,2-dimethyl-1-amino-5-hexene

Downstream raw materials:

benzyl 3-(benzyloxycarbonylimino)-6,6-dimethylhexahydroimidazo[1,5-a]pyridine-2(1H)-carboxylate