C₁₅H₂₀NO₄PS

Base Information

Chemical Name:C₁₅H₂₀NO₄PS
CAS No.:1356965-59-7
Molecular Formula:C₁₅H₂₀NO₄PS
Molecular Weight:341.368
Hs Code.:

C<sub>15</sub>H<sub>20</sub>NO<sub>4</sub>PS

Synonyms:C₁₅H₂₀NO₄PS

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₂₀NO₄PS

Chemical Property:

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Technology Process of C₁₅H₂₀NO₄PS

There total 2 articles about C₁₅H₂₀NO₄PS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: (3-cyanophenyl)magnesium bromide

: 1356965-39-3
C₁₀H₂₂NO₅PS

: 1356965-59-7
C₁₅H₂₀NO₄PS

Guidance literature:: In tetrahydrofuran; at -78 - 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ja210758n

Reference yield:

: 1356965-38-2
C₉H₁₉O₅PS

: 1356965-59-7
C₁₅H₂₀NO₄PS

Guidance literature:: Multi-step reaction with 2 steps

1: isopropyl magnesium chloride - lithium chloride complex / tetrahydrofuran / 0.33 h / -20 °C / Inert atmosphere

2: tetrahydrofuran / 3 h / -78 - 20 °C / Inert atmosphere

With isopropyl magnesium chloride - lithium chloride complex; In tetrahydrofuran;
DOI:10.1021/ja210758n

Reference yield: 83.0%

: 1356965-59-7
C₁₅H₂₀NO₄PS

: 1356965-75-7
C₁₅H₂₂NO₄PS

Guidance literature:: With borane-THF; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; at 0 ℃; Inert atmosphere;
DOI:10.1021/ja210758n