4-((E)-2-(benzo[d]thiazol-2-yl)vinyl)-N-(4-((E)-2-(benzo[d]thiazol-2-yl)vinyl)phenyl)-N-phenylaniline

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Chemical Name:4-((E)-2-(benzo[d]thiazol-2-yl)vinyl)-N-(4-((E)-2-(benzo[d]thiazol-2-yl)vinyl)phenyl)-N-phenylaniline
CAS No.:1016164-02-5
Molecular Formula:C₃₆H₂₅N₃S₂
Molecular Weight:563.747
Hs Code.:

Synonyms:4-((E)-2-(benzo[d]thiazol-2-yl)vinyl)-N-(4-((E)-2-(benzo[d]thiazol-2-yl)vinyl)phenyl)-N-phenylaniline

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Chemical Property of 4-((E)-2-(benzo[d]thiazol-2-yl)vinyl)-N-(4-((E)-2-(benzo[d]thiazol-2-yl)vinyl)phenyl)-N-phenylaniline

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Technology Process of 4-((E)-2-(benzo[d]thiazol-2-yl)vinyl)-N-(4-((E)-2-(benzo[d]thiazol-2-yl)vinyl)phenyl)-N-phenylaniline

There total 2 articles about 4-((E)-2-(benzo[d]thiazol-2-yl)vinyl)-N-(4-((E)-2-(benzo[d]thiazol-2-yl)vinyl)phenyl)-N-phenylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1628-51-9
benzothiazol-2-ylmethyl-phosphonic acid diethyl ester

: 53566-95-3
4,4'-diformyltriphenylamine

: 1016164-02-5
4-((E)-2-(benzo[d]thiazol-2-yl)vinyl)-N-(4-((E)-2-(benzo[d]thiazol-2-yl)vinyl)phenyl)-N-phenylaniline

Guidance literature:: With 15-crown-5; sodium hydride; In tetrahydrofuran; for 70h;
DOI:10.1021/jo702002y

Reference yield:

: 603-34-9
N,N-diphenylaminobenzene

: 1016164-02-5
4-((E)-2-(benzo[d]thiazol-2-yl)vinyl)-N-(4-((E)-2-(benzo[d]thiazol-2-yl)vinyl)phenyl)-N-phenylaniline

Guidance literature:: Multi-step reaction with 3 steps

1: trichlorophosphate / chloroform / 13 h / 0 - 80 °C / Inert atmosphere

2: potassium tert-butylate / 24 h / 20 °C / Inert atmosphere

3: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 120 °C / Inert atmosphere

With potassium tert-butylate; toluene-4-sulfonic acid; trichlorophosphate; In chloroform; N,N-dimethyl-formamide;
DOI:10.1039/c5tb00940e