C₁₅H₁₆N₂O₈

Base Information

Chemical Name:C₁₅H₁₆N₂O₈
CAS No.:1343407-31-7
Molecular Formula:C₁₅H₁₆N₂O₈
Molecular Weight:352.301
Hs Code.:

C<sub>15</sub>H<sub>16</sub>N<sub>2</sub>O<sub>8</sub>

Synonyms:C₁₅H₁₆N₂O₈

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Chemical Property of C₁₅H₁₆N₂O₈

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Technology Process of C₁₅H₁₆N₂O₈

There total 1 articles about C₁₅H₁₆N₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: C₁₅H₁₈N₂O₈

: 1343407-31-7
C₁₅H₁₆N₂O₈

Guidance literature:: With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trichloroisocyanuric acid; In dichloromethane; at 0 ℃;

Reference yield: 55.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 1343407-31-7
C₁₅H₁₆N₂O₈

: 1343407-32-8
C₁₆H₁₅F₃N₂O₁₀S

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at -45 - 40 ℃; for 1h; Inert atmosphere;

Reference yield:

: 1343407-31-7
C₁₅H₁₆N₂O₈

: 1343407-41-9
C₅₉H₆₉N₇O₁₄

Guidance literature:: Multi-step reaction with 9 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 1 h / -45 - 40 °C / Inert atmosphere

2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / Inert atmosphere

3.1: lithium borohydride; ethanol / tetrahydrofuran / 1 h / 15 - 25 °C / Cooling with ice

4.1: zinc; acetic acid / ethanol / 0.08 h / Reflux

5.1: triethylamine / tetrahydrofuran / 0.17 h / 0 °C

5.2: 20 - 65 °C

6.1: potassium carbonate / water; methanol / 0.83 h / 20 °C

7.1: Dess-Martin periodane / dichloromethane / 6.5 h / 20 °C

8.1: pyrrolidine / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

9.1: N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline / dichloromethane; methanol / 24 h / 20 °C

With pyrrolidine; 2,6-dimethylpyridine; lithium borohydride; ethanol; sodium carbonate; potassium carbonate; Dess-Martin periodane; acetic acid; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; triethylamine; zinc; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene; 2.1: Suzuki Coupling;