(3α, 4β, 5α)-dihydro-5(3,4-dimethoxyphenyl)-3,4-di(carboxymethyl)-2(3H)-furanone

Base Information

Chemical Name:(3α, 4β, 5α)-dihydro-5(3,4-dimethoxyphenyl)-3,4-di(carboxymethyl)-2(3H)-furanone
CAS No.:121587-94-8
Molecular Formula:C₁₆H₁₈O₈
Molecular Weight:338.314
Hs Code.:

Synonyms:(3α, 4β, 5α)-dihydro-5(3,4-dimethoxyphenyl)-3,4-di(carboxymethyl)-2(3H)-furanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3α, 4β, 5α)-dihydro-5(3,4-dimethoxyphenyl)-3,4-di(carboxymethyl)-2(3H)-furanone

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Technology Process of (3α, 4β, 5α)-dihydro-5(3,4-dimethoxyphenyl)-3,4-di(carboxymethyl)-2(3H)-furanone

There total 1 articles about (3α, 4β, 5α)-dihydro-5(3,4-dimethoxyphenyl)-3,4-di(carboxymethyl)-2(3H)-furanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 5396-64-5
methyl (E)-3-(3,4-dimethoxyphenyl)acrylate

: 38330-80-2
monomethyl monopotassium malonate

: 121587-94-8
(3α, 4β, 5α)-dihydro-5(3,4-dimethoxyphenyl)-3,4-di(carboxymethyl)-2(3H)-furanone

Guidance literature:: With manganese triacetate; acetic acid; at 70 ℃;
DOI:10.1515/HC.2003.9.3.225

Reference yield: 64.0%

: 121587-94-8
(3α, 4β, 5α)-dihydro-5(3,4-dimethoxyphenyl)-3,4-di(carboxymethyl)-2(3H)-furanone

: 3535-37-3
3,4-dimethoxybenzoic acid chloride

: (3R,4S,5S)-3-(3,4-Dimethoxy-benzoyl)-5-(3,4-dimethoxy-phenyl)-2-oxo-tetrahydro-furan-3,4-dicarboxylic acid dimethyl ester

Guidance literature:: (3α, 4β, 5α)-dihydro-5(3,4-dimethoxyphenyl)-3,4-di(carboxymethyl)-2(3H)-furanone; With sodium hydride; In tetrahydrofuran; at 20 ℃;

3,4-dimethoxybenzoic acid chloride; In tetrahydrofuran; at 20 ℃; for 6h;
DOI:10.1515/HC.2003.9.3.225

Reference yield:

: 121587-94-8
(3α, 4β, 5α)-dihydro-5(3,4-dimethoxyphenyl)-3,4-di(carboxymethyl)-2(3H)-furanone

: (2S,3S)-2,5-Bis-(3,4-dimethoxy-phenyl)-2,3-dihydro-furan-3,4-dicarboxylic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / tetrahydrofuran / 20 °C

1.2: 64 percent / tetrahydrofuran / 6 h / 20 °C

2.1: 80 percent / SnCl₄ / CH₂Cl₂ / 2 h / 20 °C

With tin(IV) chloride; sodium hydride; In tetrahydrofuran; dichloromethane;
DOI:10.1515/HC.2003.9.3.225