2-(acryloyloxy)ethyl 3,4-bis(2-phenylethynyl)benzoate

Base Information

Chemical Name:2-(acryloyloxy)ethyl 3,4-bis(2-phenylethynyl)benzoate
CAS No.:1351489-02-5
Molecular Formula:C₂₈H₂₀O₄
Molecular Weight:420.464
Hs Code.:

Synonyms:2-(acryloyloxy)ethyl 3,4-bis(2-phenylethynyl)benzoate

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Chemical Property of 2-(acryloyloxy)ethyl 3,4-bis(2-phenylethynyl)benzoate

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Technology Process of 2-(acryloyloxy)ethyl 3,4-bis(2-phenylethynyl)benzoate

There total 3 articles about 2-(acryloyloxy)ethyl 3,4-bis(2-phenylethynyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 851015-43-5
3,4-bis(2-phenylethynyl)benzoic acid

: 818-61-1,9051-31-4,26022-14-0
2-hydroxyethyl acrylate

: 1351489-02-5
2-(acryloyloxy)ethyl 3,4-bis(2-phenylethynyl)benzoate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1002/pola.25013

Reference yield:

: 51329-16-9
3,4-dibromobenzoic acid methyl ester

: 1351489-02-5
2-(acryloyloxy)ethyl 3,4-bis(2-phenylethynyl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; potassium iodide / N,N-dimethyl-formamide / Inert atmosphere

1.2: 80 °C / Inert atmosphere

2.1: sodium hydroxide / methanol; dichloromethane / 0.25 h / Inert atmosphere

2.2: pH 2 - 3 / Inert atmosphere

3.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; potassium iodide; sodium hydroxide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/pola.25013

Reference yield:

: 536-74-3
phenylacetylene

: 1351489-02-5
2-(acryloyloxy)ethyl 3,4-bis(2-phenylethynyl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; potassium iodide / N,N-dimethyl-formamide / Inert atmosphere

1.2: 80 °C / Inert atmosphere

2.1: sodium hydroxide / methanol; dichloromethane / 0.25 h / Inert atmosphere

2.2: pH 2 - 3 / Inert atmosphere

3.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; potassium iodide; sodium hydroxide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/pola.25013