2-geranyl-3,5-dimethoxy-2′-prenyl-3′-(methoxymethoxy)-4′-methoxy-(E)-stilbene

Base Information

Chemical Name:2-geranyl-3,5-dimethoxy-2′-prenyl-3′-(methoxymethoxy)-4′-methoxy-(E)-stilbene
CAS No.:1542214-47-0
Molecular Formula:C₃₄H₄₆O₅
Molecular Weight:534.736
Hs Code.:

Synonyms:2-geranyl-3,5-dimethoxy-2′-prenyl-3′-(methoxymethoxy)-4′-methoxy-(E)-stilbene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-geranyl-3,5-dimethoxy-2′-prenyl-3′-(methoxymethoxy)-4′-methoxy-(E)-stilbene

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Technology Process of 2-geranyl-3,5-dimethoxy-2′-prenyl-3′-(methoxymethoxy)-4′-methoxy-(E)-stilbene

There total 7 articles about 2-geranyl-3,5-dimethoxy-2′-prenyl-3′-(methoxymethoxy)-4′-methoxy-(E)-stilbene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 1542214-36-7
diethyl{[4-methoxy-3-(methoxymethoxy)-2-(prenyl)-phenyl]methyl} phosphonate

: 1542214-34-5
2-geranyl-3,5-dimethoxybenzaldehyde

: 1542214-47-0
2-geranyl-3,5-dimethoxy-2′-prenyl-3′-(methoxymethoxy)-4′-methoxy-(E)-stilbene

Guidance literature:: With 15-crown-5; sodium hydride; In tetrahydrofuran; mineral oil; Inert atmosphere;
DOI:10.1021/np4009046

Reference yield:

: 160624-21-5
C₁₅H₂₀O₄

: 1542214-47-0
2-geranyl-3,5-dimethoxy-2′-prenyl-3′-(methoxymethoxy)-4′-methoxy-(E)-stilbene

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / methanol / 0.5 h / 0 °C / Inert atmosphere

2: methanesulfonyl chloride; triethylamine; lithium bromide / tetrahydrofuran / Inert atmosphere

3: sodium hydride; 15-crown-5 / tetrahydrofuran; mineral oil / Inert atmosphere

With sodium tetrahydroborate; 15-crown-5; sodium hydride; methanesulfonyl chloride; triethylamine; lithium bromide; In tetrahydrofuran; methanol; mineral oil;
DOI:10.1021/np4009046

Reference yield:

: 1542214-56-1
C₁₅H₂₂O₄

: 1542214-47-0
2-geranyl-3,5-dimethoxy-2′-prenyl-3′-(methoxymethoxy)-4′-methoxy-(E)-stilbene

Guidance literature:: Multi-step reaction with 2 steps

1: methanesulfonyl chloride; triethylamine; lithium bromide / tetrahydrofuran / Inert atmosphere

2: sodium hydride; 15-crown-5 / tetrahydrofuran; mineral oil / Inert atmosphere

With 15-crown-5; sodium hydride; methanesulfonyl chloride; triethylamine; lithium bromide; In tetrahydrofuran; mineral oil;
DOI:10.1021/np4009046