2-allyl-2-carboisobutoxycyclohexanone

Base Information

Chemical Name:2-allyl-2-carboisobutoxycyclohexanone
CAS No.:692779-67-2
Molecular Formula:C₁₄H₂₂O₃
Molecular Weight:238.327
Hs Code.:

Synonyms:2-allyl-2-carboisobutoxycyclohexanone

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Chemical Property of 2-allyl-2-carboisobutoxycyclohexanone

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Technology Process of 2-allyl-2-carboisobutoxycyclohexanone

There total 3 articles about 2-allyl-2-carboisobutoxycyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 106-95-6
allyl bromide

: 298204-46-3
isobutyl 2-oxocyclohexanecarboxylate

: 692779-67-2
2-allyl-2-carboisobutoxycyclohexanone

Guidance literature:: isobutyl 2-oxocyclohexanecarboxylate; With potassium carbonate; In acetone; at 20 ℃; for 0.5h;

allyl bromide; In acetone; at 20 ℃; for 24h; Further stages.;
DOI:10.1016/j.tet.2004.01.079

Reference yield:

: 111-16-0
heptanedioic acid

: 692779-67-2
2-allyl-2-carboisobutoxycyclohexanone

Guidance literature:: Multi-step reaction with 3 steps

1.1: 82 percent / sulfuric acid / 8 h / Heating

2.1: 95 percent / AlCl₃; Et₃N / CH₂Cl₂ / 0 - 20 °C

3.1: K₂CO₃ / acetone / 0.5 h / 20 °C

3.2: 88 percent / acetone / 24 h / 20 °C

With aluminium trichloride; sulfuric acid; potassium carbonate; triethylamine; In dichloromethane; acetone; 2.1: Dieckmann cyclization;
DOI:10.1016/j.tet.2004.01.079

Reference yield:

: 40775-17-5
diisobutyl pimelate

: 692779-67-2
2-allyl-2-carboisobutoxycyclohexanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: 95 percent / AlCl₃; Et₃N / CH₂Cl₂ / 0 - 20 °C

2.1: K₂CO₃ / acetone / 0.5 h / 20 °C

2.2: 88 percent / acetone / 24 h / 20 °C

With aluminium trichloride; potassium carbonate; triethylamine; In dichloromethane; acetone; 1.1: Dieckmann cyclization;
DOI:10.1016/j.tet.2004.01.079