N-(1-dimethylaminoethylene)-4-(5H,11H-pyrrolo[2,1-c][1,4]benzodiazepine-10-carbonyl)-benzamide

Base Information

• Chemical Name: N-(1-dimethylaminoethylene)-4-(5H,11H-pyrrolo[2,1-c][1,4]benzodiazepine-10-carbonyl)-benzamide
• CAS No.: 220461-80-3
• Molecular Formula: C₂₄H₂₄N₄O₂
• Molecular Weight: 400.48

Synonyms:N-(1-dimethylaminoethylene)-4-(5H,11H-pyrrolo[2,1-c][1,4]benzodiazepine-10-carbonyl)-benzamide

Chemical Property of N-(1-dimethylaminoethylene)-4-(5H,11H-pyrrolo[2,1-c][1,4]benzodiazepine-10-carbonyl)-benzamide

Chemical Property:

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Technology Process of N-(1-dimethylaminoethylene)-4-(5H,11H-pyrrolo[2,1-c][1,4]benzodiazepine-10-carbonyl)-benzamide

There total 2 articles about N-(1-dimethylaminoethylene)-4-(5H,11H-pyrrolo[2,1-c][1,4]benzodiazepine-10-carbonyl)-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-dimethylacetamide dimethyl acetal (18871-66-4) + 4-(5H,11H-Pyrrolo[2,1-c][1,4]benzodiazepine-10-carbonyl)-benzamide (220461-78-9) → N-(1-dimethylaminoethylene)-4-(5H,11H-pyrrolo[2,1-c][1,4]benzodiazepine-10-carbonyl)-benzamide (220461-80-3)

Guidance literature:

for 4h; Heating / reflux;

Reference yield:

4-(5H,11H-Pyrrolo[2,1-c][1,41]benzodiazepine-10-carbonyl)-benzamide + N,N-dimethylacetamide dimethyl acetal (18871-66-4) + 4-(5H,11H-Pyrrolo[2,1-c][1,4]benzodiazepine-10-carbonyl)-benzamide (220461-78-9) → N-(1-dimethylaminoethylene)-4-(5H,11H-pyrrolo[2,1-c][1,4]benzodiazepine-10-carbonyl)-benzamide (220461-80-3)

Guidance literature:

Reference yield:

N-(1-dimethylaminoethylene)-4-(5H,11H-pyrrolo[2,1-c][1,4]benzodiazepine-10-carbonyl)-benzamide (220461-80-3) → [4-(3-Methyl[1,2,4]oxadiazol-5-yl)-phenyl]-(5H,11H-pyrrolo-[2,1-c][1,4]-benzodiazepin-10-yl)-methanone (220461-28-9)

Guidance literature:

With hydroxylamine hydrochloride; potassium acetate; sodium hydrogencarbonate; In hexane; acetic acid;

upstream raw materials:

N,N-dimethylacetamide dimethyl acetal

4-(5H,11H-Pyrrolo[2,1-c][1,4]benzodiazepine-10-carbonyl)-benzamide

Downstream raw materials:

[4-(2,5-Dimethyl-2H-[1,2,4]triazol-3-yl)-phenyl]-(5H,11H-pyrrolo[2,1-c]-[1,4]benzodiazepin-10-yl)-methanone

[4-(5-Methyl-2H-[1,2,4]triazol-3-yl)-phenyl]-(5H,11H-pyrrolo[2,1-c][1,4]-benzodiazepin-10-yl)-methanone

[4-(3-Methyl[1,2,4]oxadiazol-5-yl)-phenyl]-(5H,11H-pyrrolo-[2,1-c][1,4]-benzodiazepin-10-yl)-methanone

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