1-(4-Bromobenzenesulfonyl)-2-methoxycarbonylsulfenyl-1-methylhydrazine

Base Information

Chemical Name:1-(4-Bromobenzenesulfonyl)-2-methoxycarbonylsulfenyl-1-methylhydrazine
CAS No.:102235-40-5
Molecular Formula:C₉H₁₁BrN₂O₄S₂
Molecular Weight:355.233
Hs Code.:

Synonyms:1-(4-Bromobenzenesulfonyl)-2-methoxycarbonylsulfenyl-1-methylhydrazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-Bromobenzenesulfonyl)-2-methoxycarbonylsulfenyl-1-methylhydrazine

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Technology Process of 1-(4-Bromobenzenesulfonyl)-2-methoxycarbonylsulfenyl-1-methylhydrazine

There total 3 articles about 1-(4-Bromobenzenesulfonyl)-2-methoxycarbonylsulfenyl-1-methylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 26555-40-8
metgoxycarbonylsulfenyl chloride

: 102235-41-6
1-<(4-bromomethylphenyl)sulfonyl>-1-methylhydrazine

: 102235-40-5
1-(4-Bromobenzenesulfonyl)-2-methoxycarbonylsulfenyl-1-methylhydrazine

Guidance literature:: With pyridine; In diethyl ether; at 0 - 5 ℃; for 0.25h;
DOI:10.1021/jm00159a036

Reference yield:

: 98-58-8
4-bromobenzenesulfonyl chloride

: 102235-40-5
1-(4-Bromobenzenesulfonyl)-2-methoxycarbonylsulfenyl-1-methylhydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / tetrahydrofuran / 4 h / 0 - 5 °C

2: 79 percent / pyridine / diethyl ether / 0.25 h / 0 - 5 °C

With pyridine; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jm00159a036