(E)-3-(2-Methoxyphenyl)-2-propenylamine

Base Information

• Chemical Name: (E)-3-(2-Methoxyphenyl)-2-propenylamine
• CAS No.: 158223-63-3
• Molecular Formula: C₁₀H₁₃NO
• Molecular Weight: 163.219
• Mol file: 158223-63-3.mol

Synonyms:(E)-3-(2-Methoxyphenyl)-2-propenylamine

Chemical Property of (E)-3-(2-Methoxyphenyl)-2-propenylamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (E)-3-(2-Methoxyphenyl)-2-propenylamine

There total 4 articles about (E)-3-(2-Methoxyphenyl)-2-propenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-3-(2-methoxyphenyl)propenal (60125-24-8) → (E)-3-(2-Methoxyphenyl)-2-propenylamine (158223-63-3)

Guidance literature:

With (S)-1-phenyl-ethylamine; pyridoxal 5'-phosphate; pQR₁₁₀₈; In aq. phosphate buffer; dimethyl sulfoxide; at 30 ℃; for 18h; pH=8; Enzymatic reaction;

DOI:10.1039/c6gc02769e

Reference yield:

(E)-3-(2-methoxyphenyl)prop-2-en-1-ol (1504-61-6,13523-28-9,114568-19-3) → C20H23NO2 + (E)-3-(2-Methoxyphenyl)-2-propenylamine (158223-63-3)

Guidance literature:

With dichloro(1,5-cyclooctadiene)platinum(ll); ammonium hydroxide; bis[2-(diphenylphosphino)phenyl] ether; In 1,4-dioxane; methanol; at 100 ℃; for 48h; Inert atmosphere; Autoclave;

DOI:10.1002/anie.201106737

Reference yield:

ortho-anisaldehyde (135-02-4) + 1-Aza-1,3-bis(triphenylphosphoranylidene)propane (1061242-67-8) → (Z)-3-(2-Methoxyphenyl)-2-propenylamine + (E)-3-(2-Methoxyphenyl)-2-propenylamine (158223-63-3)

Guidance literature:

In tetrahydrofuran; hexane; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;

DOI:10.1021/jo00095a034

upstream raw materials:

ortho-anisaldehyde

1-Aza-1,3-bis(triphenylphosphoranylidene)propane

(E)-3-(2-methoxyphenyl)prop-2-en-1-ol

(E)-3-(2-methoxyphenyl)propenal

Downstream raw materials:

(E)-1-methoxy-2-(3-(phenylsulfonyl)prop-1-en-1-yl)benzene