2,5-bis(2-ethylhexyl)-3,6-bis(5-(4-methoxyphenyl)thiophen-2-yl)-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione

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Chemical Name:2,5-bis(2-ethylhexyl)-3,6-bis(5-(4-methoxyphenyl)thiophen-2-yl)-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione
CAS No.:1401967-47-2
Molecular Formula:C₄₄H₅₂N₂O₄S₂
Molecular Weight:737.04
Hs Code.:

Synonyms:2,5-bis(2-ethylhexyl)-3,6-bis(5-(4-methoxyphenyl)thiophen-2-yl)-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione

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Chemical Property of 2,5-bis(2-ethylhexyl)-3,6-bis(5-(4-methoxyphenyl)thiophen-2-yl)-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione

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Technology Process of 2,5-bis(2-ethylhexyl)-3,6-bis(5-(4-methoxyphenyl)thiophen-2-yl)-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione

There total 2 articles about 2,5-bis(2-ethylhexyl)-3,6-bis(5-(4-methoxyphenyl)thiophen-2-yl)-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 104-92-7
1-bromo-4-methoxy-benzene

: 1185885-86-2
2,5-bis(2-ethylhexyl)-3,6-di(thiophen-2-yl)pyrrolo[3,4-c]pyrrole-1,4-dione

: 1401967-47-2
2,5-bis(2-ethylhexyl)-3,6-bis(5-(4-methoxyphenyl)thiophen-2-yl)-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione

Guidance literature:: 2,5-bis(2-ethylhexyl)-3,6-di(thiophen-2-yl)pyrrolo[3,4-c]pyrrole-1,4-dione; With palladium diacetate; potassium carbonate; Trimethylacetic acid; for 0.5h; Inert atmosphere;

1-bromo-4-methoxy-benzene; With N,N-dimethyl acetamide; at 100 ℃; for 3h; Inert atmosphere;
DOI:10.1039/c2jm35398a

Reference yield: 51.0%

: 1185885-86-2
2,5-bis(2-ethylhexyl)-3,6-di(thiophen-2-yl)pyrrolo[3,4-c]pyrrole-1,4-dione

: 696-62-8
para-iodoanisole

: 1401967-47-2
2,5-bis(2-ethylhexyl)-3,6-bis(5-(4-methoxyphenyl)thiophen-2-yl)-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tris(o-methoxyphenyl)phosphine; caesium carbonate; Trimethylacetic acid; In neat (no solvent); at 110 ℃; for 15h; Schlenk technique; Sealed tube; Green chemistry;
DOI:10.1021/acs.joc.8b01284