4,10-bis-(toluene-4-sulfonyl)-1,4,7,10-tetraaza-bicyclo[5.5.2]tetradecane

Base Information

• Chemical Name: 4,10-bis-(toluene-4-sulfonyl)-1,4,7,10-tetraaza-bicyclo[5.5.2]tetradecane
• CAS No.: 226917-74-4
• Molecular Formula: C₂₄H₃₄N₄O₄S₂
• Molecular Weight: 506.69

Synonyms:4,10-bis-(toluene-4-sulfonyl)-1,4,7,10-tetraaza-bicyclo[5.5.2]tetradecane

Chemical Property of 4,10-bis-(toluene-4-sulfonyl)-1,4,7,10-tetraaza-bicyclo[5.5.2]tetradecane

Chemical Property:

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Technology Process of 4,10-bis-(toluene-4-sulfonyl)-1,4,7,10-tetraaza-bicyclo[5.5.2]tetradecane

There total 4 articles about 4,10-bis-(toluene-4-sulfonyl)-1,4,7,10-tetraaza-bicyclo[5.5.2]tetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

4,10-bis-(toluene-4-sulfonyl)-1,4,7,10-tetraaza-bicyclo[5.5.2]tetradecane-2,6-dione (226917-73-3) → 4,10-bis-(toluene-4-sulfonyl)-1,4,7,10-tetraaza-bicyclo[5.5.2]tetradecane (226917-74-4)

Guidance literature:

With borane-THF; In dichloromethane;

DOI:10.1002/(SICI)1521-3773(19990401)38:7<956::AID-ANIE956>3.0.CO;2-K

Reference yield:

N-Tosyliminodiacetic acid dichloroanhydride (42031-77-6) → 4,10-bis-(toluene-4-sulfonyl)-1,4,7,10-tetraaza-bicyclo[5.5.2]tetradecane (226917-74-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 43 percent / Ca(OH)2; molecular sieves 4 Angstroem / xylene / 6 h / Heating

2: 75 percent / BH₃*THF / CH₂Cl₂

With calcium hydroxide; borane-THF; 4 A molecular sieve; In dichloromethane; xylene; 1: Acylation / 2: Reduction;

DOI:10.1002/(SICI)1521-3773(19990401)38:7<956::AID-ANIE956>3.0.CO;2-K

Reference yield:

1-(p-toluenesulfonyl)-1,4,7-triazacyclononane (129422-96-4) → 4,10-bis-(toluene-4-sulfonyl)-1,4,7,10-tetraaza-bicyclo[5.5.2]tetradecane (226917-74-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 43 percent / Ca(OH)2; molecular sieves 4 Angstroem / xylene / 6 h / Heating

2: 75 percent / BH₃*THF / CH₂Cl₂

With calcium hydroxide; borane-THF; 4 A molecular sieve; In dichloromethane; xylene; 1: Acylation / 2: Reduction;

DOI:10.1002/(SICI)1521-3773(19990401)38:7<956::AID-ANIE956>3.0.CO;2-K

upstream raw materials:

4,10-bis-(toluene-4-sulfonyl)-1,4,7,10-tetraaza-bicyclo[5.5.2]tetradecane-2,6-dione

N-Tosyliminodiacetic acid dichloroanhydride

1-(p-toluenesulfonyl)-1,4,7-triazacyclononane

N,N',N-tris(p-toluenesulfonyl)-1,4,7-triazacyclononane

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