1,5-dihydro-3-methyllumiflavin

Base Information

• Chemical Name: 1,5-dihydro-3-methyllumiflavin
• CAS No.: 23542-57-6
• Molecular Formula: C₁₄H₁₆N₄O₂
• Molecular Weight: 272.307
• Mol file: 23542-57-6.mol

Synonyms:1,5-dihydro-3-methyllumiflavin

Chemical Property of 1,5-dihydro-3-methyllumiflavin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 1,5-dihydro-3-methyllumiflavin

There total 6 articles about 1,5-dihydro-3-methyllumiflavin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

N-benzyl-N-methyl-1-(trimethylsilyl)methanamine (51951-99-6) + 3-methyllumiflavin (18636-32-3) → 1,5-dihydro-3-methyllumiflavin (23542-57-6) + benzyl-methyl-amine (103-67-3)

Guidance literature:

With water; In [D₃]acetonitrile; for 0.166667h; Irradiation;

DOI:10.1021/jo00016a026

Reference yield:

(phenylthio)acetic acid (103-04-8) + 3-methyllumiflavin (18636-32-3) → 1,5-dihydro-3-methyllumiflavin (23542-57-6) + methyl-phenyl-thioether (100-68-5) + 3,7,8,10-Tetramethyl-4a-phenylsulfanylmethyl-5,10-dihydro-4aH-benzo[g]pteridine-2,4-dione (73644-41-4) + C14H14N4O2*H

Guidance literature:

In acetonitrile; Mechanism; Rate constant; Irradiation;

DOI:10.1021/ja00524a063

Reference yield:

N-2,3-butadienyl-N-methylbenzylamine (16719-33-8) + 3-methyllumiflavin (18636-32-3) → 1,5-dihydro-3-methyllumiflavin (23542-57-6) + C26H29N5O2 (83365-39-3)

Guidance literature:

In water; acetonitrile; Product distribution; Quantum yield; Irradiation; pH 7.2; photolyses of 3-methyllumiflavin with various amines; quenching of 3-MLF fluorescence by secondary and tertiary amines, concentration and solvent dependence;

DOI:10.1021/ja00389a044

upstream raw materials:

(phenylthio)acetic acid

3-methyllumiflavin

N-2,3-butadienyl-N-methylbenzylamine

N-benzyl-N-methyl-1-(trimethylsilyl)methanamine