triisopropylsilyl 3-[(4-{[4-(dodecyloxy)phenyl]diazenyl}benzoyl)oxy]-5-hydroxybenzoate

Base Information

Chemical Name:triisopropylsilyl 3-[(4-{[4-(dodecyloxy)phenyl]diazenyl}benzoyl)oxy]-5-hydroxybenzoate
CAS No.:1394920-98-9
Molecular Formula:C₄₁H₅₈N₂O₆Si
Molecular Weight:703.007
Hs Code.:

Synonyms:triisopropylsilyl 3-[(4-{[4-(dodecyloxy)phenyl]diazenyl}benzoyl)oxy]-5-hydroxybenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of triisopropylsilyl 3-[(4-{[4-(dodecyloxy)phenyl]diazenyl}benzoyl)oxy]-5-hydroxybenzoate

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Technology Process of triisopropylsilyl 3-[(4-{[4-(dodecyloxy)phenyl]diazenyl}benzoyl)oxy]-5-hydroxybenzoate

There total 2 articles about triisopropylsilyl 3-[(4-{[4-(dodecyloxy)phenyl]diazenyl}benzoyl)oxy]-5-hydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 703404-59-5
3,5-dihydroxy-triisopropylsilyl benzoate

: 1253388-98-5
4-{[4-(dodecyloxy)phenyl]azo}benzoyl chloride

: 1394920-98-9
triisopropylsilyl 3-[(4-{[4-(dodecyloxy)phenyl]diazenyl}benzoyl)oxy]-5-hydroxybenzoate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 15h; Inert atmosphere;
DOI:10.1039/c2jm33331g

Reference yield:

: 142747-37-3
C₂₅H₃₄N₂O₃

: 1394920-98-9
triisopropylsilyl 3-[(4-{[4-(dodecyloxy)phenyl]diazenyl}benzoyl)oxy]-5-hydroxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / dichloromethane / 2 h / 20 °C

2: triethylamine / dichloromethane / 15 h / 20 °C / Inert atmosphere

With oxalyl dichloride; triethylamine; In dichloromethane;
DOI:10.1039/c2jm33331g

Reference yield: 94.0%

: 1307908-00-4
4-{5-[4-(dodecyloxy)phenyl]-1,3,4-oxadiazol-2-yl}benzoic acid

: 1394920-98-9
triisopropylsilyl 3-[(4-{[4-(dodecyloxy)phenyl]diazenyl}benzoyl)oxy]-5-hydroxybenzoate

: triisopropylsilyl 3-[(4-{5-[4-(dodecyloxy)phenyl]-1,3,4-oxadiazol-2-yl}benzoyl)oxy]-5-[(4-{[4-(dodecyloxy)phenyl]diazenyl}benzoyl)oxy]benzoate

Guidance literature:: With dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate; In dichloromethane; at 0 - 20 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c4tc00886c