Technology Process of C41H38F2N4O12
There total 8 articles about C41H38F2N4O12 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
lithium borohydride; ethanol;
In
tetrahydrofuran; ethanol;
at 15 - 25 ℃;
for 1h;
Cooling with ice;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: trichloroisocyanuric acid; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / 0.5 h / 0 °C
2: 2,6-dimethylpyridine / dichloromethane / 1 h / -45 - 40 °C / Inert atmosphere
3: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / Inert atmosphere
4: lithium borohydride; ethanol / ethanol; tetrahydrofuran / 1 h / 15 - 25 °C / Cooling with ice
With
2,6-dimethylpyridine; lithium borohydride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; ethanol; trichloroisocyanuric acid; sodium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; ethanol; dichloromethane; water; toluene;
3: Suzuki Coupling;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 2,6-dimethylpyridine / dichloromethane / 1 h / -45 - 40 °C / Inert atmosphere
2: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / Inert atmosphere
3: lithium borohydride; ethanol / ethanol; tetrahydrofuran / 1 h / 15 - 25 °C / Cooling with ice
With
2,6-dimethylpyridine; lithium borohydride; ethanol; sodium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; ethanol; dichloromethane; water; toluene;
2: Suzuki Coupling;