C₁₂H₁₈O₄S

Base Information

Chemical Name:C₁₂H₁₈O₄S
CAS No.:1338989-87-9
Molecular Formula:C₁₂H₁₈O₄S
Molecular Weight:258.339
Hs Code.:

C<sub>12</sub>H<sub>18</sub>O<sub>4</sub>S

Synonyms:C₁₂H₁₈O₄S

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Chemical Property of C₁₂H₁₈O₄S

Chemical Property:

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Technology Process of C₁₂H₁₈O₄S

There total 7 articles about C₁₂H₁₈O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: C₁₂H₁₆O₄S

: 1338989-87-9
C₁₂H₁₈O₄S

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 25 ℃; regioselective reaction;
DOI:10.1016/j.tetlet.2011.08.051

Reference yield:

: C₁₂H₁₂O₂S

: 1338989-87-9
C₁₂H₁₈O₄S

Guidance literature:: Multi-step reaction with 6 steps

1: sodium thiophenolate / methanol / 23 °C

2: copper(l) iodide / tetrahydrofuran / -78 °C

3: diisobutylaluminium hydride / dichloromethane / 0 °C

4: hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide / ethanol / -15 °C

5: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -40 °C

6: lithium aluminium tetrahydride / tetrahydrofuran / 25 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; copper(l) iodide; lithium aluminium tetrahydride; hexaammonium heptamolybdate tetrahydrate; diethyl (2R,3R)-tartrate; dihydrogen peroxide; sodium thiophenolate; diisobutylaluminium hydride; In tetrahydrofuran; methanol; ethanol; dichloromethane; 5: Katsuki-Sharpless asymmetric epoxidation;
DOI:10.1016/j.tetlet.2011.08.051

Reference yield:

: 73311-79-2
C₁₃H₁₆O₂S

: 1338989-87-9
C₁₂H₁₈O₄S

Guidance literature:: Multi-step reaction with 4 steps

1: diisobutylaluminium hydride / dichloromethane / 0 °C

2: hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide / ethanol / -15 °C

3: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -40 °C

4: lithium aluminium tetrahydride / tetrahydrofuran / 25 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; lithium aluminium tetrahydride; hexaammonium heptamolybdate tetrahydrate; diethyl (2R,3R)-tartrate; dihydrogen peroxide; diisobutylaluminium hydride; In tetrahydrofuran; ethanol; dichloromethane; 3: Katsuki-Sharpless asymmetric epoxidation;
DOI:10.1016/j.tetlet.2011.08.051