(1E,2E)-2-{1-[(o-hydroxyphenyl)imino]-2-triisopropylsilyl-3-phenyl-2-propenyl}-3,4-dihydro-3,3,5-trimethyl-1,2-benzothiazole 1,1-dioxide

Base Information

Chemical Name:(1E,2E)-2-{1-[(o-hydroxyphenyl)imino]-2-triisopropylsilyl-3-phenyl-2-propenyl}-3,4-dihydro-3,3,5-trimethyl-1,2-benzothiazole 1,1-dioxide
CAS No.:1185039-86-4
Molecular Formula:C₃₄H₄₄N₂O₃SSi
Molecular Weight:588.886
Hs Code.:

Synonyms:(1E,2E)-2-{1-[(o-hydroxyphenyl)imino]-2-triisopropylsilyl-3-phenyl-2-propenyl}-3,4-dihydro-3,3,5-trimethyl-1,2-benzothiazole 1,1-dioxide

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Chemical Property of (1E,2E)-2-{1-[(o-hydroxyphenyl)imino]-2-triisopropylsilyl-3-phenyl-2-propenyl}-3,4-dihydro-3,3,5-trimethyl-1,2-benzothiazole 1,1-dioxide

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Technology Process of (1E,2E)-2-{1-[(o-hydroxyphenyl)imino]-2-triisopropylsilyl-3-phenyl-2-propenyl}-3,4-dihydro-3,3,5-trimethyl-1,2-benzothiazole 1,1-dioxide

There total 1 articles about (1E,2E)-2-{1-[(o-hydroxyphenyl)imino]-2-triisopropylsilyl-3-phenyl-2-propenyl}-3,4-dihydro-3,3,5-trimethyl-1,2-benzothiazole 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 1185039-57-9
2,3-dihydro-2-[2-(triisopropylsilyl)ethynyl]-3,3,5-trimethyl-1,2-benzothiazole 1,1-dioxide

: 117649-28-2
N-(4-methylbenzylidene)-o-hydroxyphenylamine

: 1185039-86-4
(1E,2E)-2-{1-[(o-hydroxyphenyl)imino]-2-triisopropylsilyl-3-phenyl-2-propenyl}-3,4-dihydro-3,3,5-trimethyl-1,2-benzothiazole 1,1-dioxide

Guidance literature:: With bis(trifluoromethanesulfonyl)amide; In 1,2-dichloro-ethane; at 60 ℃; Inert atmosphere;
DOI:10.1002/chem.200901103

Reference yield: 80.0%

: 1185039-86-4
(1E,2E)-2-{1-[(o-hydroxyphenyl)imino]-2-triisopropylsilyl-3-phenyl-2-propenyl}-3,4-dihydro-3,3,5-trimethyl-1,2-benzothiazole 1,1-dioxide

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 1185040-01-0
(1E,2E)-2-{2-triisopropyl-1-[(o-triisopropylsilyloxyphenyl)imino]-3-phenyl-2-propenyl}-3,4-dihydro-3,3,5-trimethyl-1,2-benzothiazole 1,1-dioxide

Guidance literature:: (1E,2E)-2-{1-[(o-hydroxyphenyl)imino]-2-triisopropylsilyl-3-phenyl-2-propenyl}-3,4-dihydro-3,3,5-trimethyl-1,2-benzothiazole 1,1-dioxide; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.333333h; Inert atmosphere;

triisopropylsilyl trifluoromethanesulfonate; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/chem.200901103