Technology Process of C30H28N6O3
There total 10 articles about C30H28N6O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine;
In
1-methyl-pyrrolidin-2-one;
at 150 ℃;
for 17h;
Inert atmosphere;
Microwave irradiation;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 2 h / 20 °C
1.2: 2 h / 25 - 40 °C / Cooling with ice
2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -30 - -10 °C / Inert atmosphere
2.2: 2 h / -30 - -10 °C / Inert atmosphere
2.3: 10.5 h / 20 °C
3.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C
4.1: copper(I) bromide; N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 1.5 h / 20 °C
5.1: N-ethyl-N,N-diisopropylamine / 1-methyl-pyrrolidin-2-one / 17 h / 150 °C / Inert atmosphere; Microwave irradiation
With
n-butyllithium; oxalyl dichloride; triethylamine; N-ethyl-N,N-diisopropylamine; copper(I) bromide;
In
tetrahydrofuran; 1-methyl-pyrrolidin-2-one; hexane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -30 - -10 °C / Inert atmosphere
1.2: 2 h / -30 - -10 °C / Inert atmosphere
1.3: 10.5 h / 20 °C
2.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C
3.1: copper(I) bromide; N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 1.5 h / 20 °C
4.1: N-ethyl-N,N-diisopropylamine / 1-methyl-pyrrolidin-2-one / 17 h / 150 °C / Inert atmosphere; Microwave irradiation
With
n-butyllithium; triethylamine; N-ethyl-N,N-diisopropylamine; copper(I) bromide;
In
tetrahydrofuran; 1-methyl-pyrrolidin-2-one; hexane; dichloromethane; dimethyl sulfoxide;