Technology Process of C27H30O2
There total 3 articles about C27H30O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C20H20O2;
With
hydroxylamine hydrochloride; N-butylamine; copper(l) chloride;
In
methanol;
at 0 ℃;
for 0.166667h;
Inert atmosphere;
1-bromohept-1-yne;
In
methanol;
at 0 ℃;
for 1h;
Inert atmosphere;
DOI:10.1021/jo102188q
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: dmap; 1,2-dichloro-ethane / dichloromethane / 48 h
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.17 h / 0 °C
3.1: hydroxylamine hydrochloride; N-butylamine; copper(l) chloride / methanol / 0.17 h / 0 °C / Inert atmosphere
3.2: 1 h / 0 °C / Inert atmosphere
With
dmap; hydroxylamine hydrochloride; tetrabutyl ammonium fluoride; 1,2-dichloro-ethane; N-butylamine; copper(l) chloride;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jo102188q
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: dmap; 1,2-dichloro-ethane / dichloromethane / 48 h
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.17 h / 0 °C
3.1: hydroxylamine hydrochloride; N-butylamine; copper(l) chloride / methanol / 0.17 h / 0 °C / Inert atmosphere
3.2: 1 h / 0 °C / Inert atmosphere
With
dmap; hydroxylamine hydrochloride; tetrabutyl ammonium fluoride; 1,2-dichloro-ethane; N-butylamine; copper(l) chloride;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jo102188q
