N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-3-phenyl-2-propenamide

Base Information

Chemical Name:N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-3-phenyl-2-propenamide
CAS No.:56786-05-1
Molecular Formula:C₂₈H₃₀N₂O₁₀
Molecular Weight:554.554
Hs Code.:

N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-3-phenyl-2-propenamide

Synonyms:N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-3-phenyl-2-propenamide

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Chemical Property of N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-3-phenyl-2-propenamide

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Technology Process of N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-3-phenyl-2-propenamide

There total 5 articles about N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-3-phenyl-2-propenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1489284-85-6
C₃₀H₃₂N₂O₁₁

: 56786-05-1
N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-3-phenyl-2-propenamide

Guidance literature:: With sodium cyanide; In methanol; at 25 ℃;
DOI:10.1016/j.bmc.2013.06.042

Reference yield:

: 116635-17-7
1-<(2,6-dimethyl-4-oxo-4H-<1>benzopyrano<3,4-d>oxazol-7-yl)oxy>-2-acetoxy-4-methoxy-5,5-dimethyl-3-tetrahydropyranyl 5-methyl-1H-pyrrole-2-carboxylate

: 56786-05-1
N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-3-phenyl-2-propenamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethanol / 3 h / Reflux

2.1: dicyclohexyl-carbodiimide; 4-pyrrolidin-1-ylpyridine / ethanol / 0.5 h / 25 °C

2.2: 25 °C

3.1: sodium cyanide / methanol / 25 °C

With sodium cyanide; 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide; In methanol; ethanol;
DOI:10.1016/j.bmc.2013.06.042

Reference yield:

: 1476-53-5,6990-02-9,18656-99-0
sodium novobiocin

: 56786-05-1
N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-3-phenyl-2-propenamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogenchloride / water

2.1: pyridine / 24 h / Reflux

3.1: ethanol / 3 h / Reflux

4.1: dicyclohexyl-carbodiimide; 4-pyrrolidin-1-ylpyridine / ethanol / 0.5 h / 25 °C

4.2: 25 °C

5.1: sodium cyanide / methanol / 25 °C

With pyridine; hydrogenchloride; sodium cyanide; 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide; In methanol; ethanol; water;
DOI:10.1016/j.bmc.2013.06.042