C₂₅H₃₅BrN₂O₆

Base Information

Chemical Name:C₂₅H₃₅BrN₂O₆
CAS No.:1357622-89-9
Molecular Formula:C₂₅H₃₅BrN₂O₆
Molecular Weight:539.467
Hs Code.:

C<sub>25</sub>H<sub>35</sub>BrN<sub>2</sub>O<sub>6</sub>

Synonyms:C₂₅H₃₅BrN₂O₆

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Chemical Property of C₂₅H₃₅BrN₂O₆

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Technology Process of C₂₅H₃₅BrN₂O₆

There total 18 articles about C₂₅H₃₅BrN₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1357622-65-1
C₃₁H₄₉BrN₂O₆Si

: 1357622-89-9
C₂₅H₃₅BrN₂O₆

Guidance literature:: With hydrogen fluoride; In water; acetonitrile; at -10 ℃;
DOI:10.1039/c1ob06632c

Reference yield:

: 873550-75-5
(2R,3R)-4-azido-2,3-O-isopropylidene-2,3-dihydroxybutanal

: 1357622-89-9
C₂₅H₃₅BrN₂O₆

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine / tetrahydrofuran / 50 °C / Inert atmosphere; Molecular sieve

2: methanol / 48 h / 20 °C / Inert atmosphere; Molecular sieve

3: hydrogen fluoride / water; acetonitrile / -10 °C

With hydrogen fluoride; triphenylphosphine; In tetrahydrofuran; methanol; water; acetonitrile; 2: Ugi condensation;
DOI:10.1039/c1ob06632c

Reference yield:

: 873550-74-4
(2S,3R)-4-azido-2,3-O-isopropylidene-1,2,3-butanetriol

: 1357622-89-9
C₂₅H₃₅BrN₂O₆

Guidance literature:: Multi-step reaction with 4 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -70 °C / Inert atmosphere

1.2: 1 h / -70 - -60 °C / Inert atmosphere

2.1: triphenylphosphine / tetrahydrofuran / 50 °C / Inert atmosphere; Molecular sieve

3.1: methanol / 48 h / 20 °C / Inert atmosphere; Molecular sieve

4.1: hydrogen fluoride / water; acetonitrile / -10 °C

With oxalyl dichloride; hydrogen fluoride; dimethyl sulfoxide; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile; 1.1: Swern oxidation / 1.2: Swern oxidation / 3.1: Ugi condensation;
DOI:10.1039/c1ob06632c