Technology Process of C19H25FIN3O2S
There total 6 articles about C19H25FIN3O2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N-iodo-succinimide;
In
1,4-dioxane;
at 80 ℃;
for 0.5h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrazine hydrate / methanol / 1 h / 20 °C
2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 3 h / Reflux
3: potassium phosphate; potassium bromide / tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane / 0.5 h / 160 °C / Microwave irradiation; Sealed tube
4: N-iodo-succinimide / 1,4-dioxane / 0.5 h / 80 °C
With
potassium phosphate; N-iodo-succinimide; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; potassium bromide;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; 1,4-dioxane; methanol;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C
2.1: 1-methyl-1H-imidazole / titanium tetrachloride / dichloromethane / 0.5 h / -60 °C
2.2: 0.67 h / -40 °C
3.1: hydrazine hydrate / methanol / 1 h / 20 °C
4.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 3 h / Reflux
5.1: potassium phosphate; potassium bromide / tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane / 0.5 h / 160 °C / Microwave irradiation; Sealed tube
6.1: N-iodo-succinimide / 1,4-dioxane / 0.5 h / 80 °C
With
1-methyl-1H-imidazole; potassium phosphate; N-iodo-succinimide; oxalyl dichloride; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; potassium bromide;
tetrakis(triphenylphosphine) palladium(0); titanium tetrachloride; N,N-dimethyl-formamide;
In
tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane;