12-amino-12-oxododecanoic acid

Base Information

• Chemical Name: 12-amino-12-oxododecanoic acid
• CAS No.: 21842-33-1
• Molecular Formula: C₁₂H₂₃NO₃
• Molecular Weight: 229.32
• Mol file: 21842-33-1.mol

Synonyms:12-amino-12-oxododecanoic acid

Chemical Property of 12-amino-12-oxododecanoic acid

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 12-amino-12-oxododecanoic acid

There total 1 articles about 12-amino-12-oxododecanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2-azacyclotridecanone (947-04-6,25038-74-8) → dodecandioic imide (21903-43-5) + 12-amino-12-oxododecanoic acid (21842-33-1) + 12-nitrododecanoic acid (32571-74-7)

Guidance literature:

With methyltrifluoromethyldioxirane; trifluoroacetic acid; In acetone; at 0 ℃; for 3h;

DOI:10.1002/chem.201604507

Reference yield:

12-amino-12-oxododecanoic acid (21842-33-1) → 11-aminoundecanoic acid (2432-99-7,25587-80-8,84029-94-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / bromine / methanol / 0.25 h / 70 - 80 °C

2: 34 percent / aq. NaOH / ethanol / 17 h / Heating

With sodium hydroxide; bromine; In methanol; ethanol;

DOI:10.1007/s11746-997-0176-z

upstream raw materials:

2-azacyclotridecanone

Downstream raw materials:

11-aminoundecanoic acid

Refernces