C₁₄H₁₄F₃NO₃

Base Information

Chemical Name:C₁₄H₁₄F₃NO₃
CAS No.:1234790-98-7
Molecular Formula:C₁₄H₁₄F₃NO₃
Molecular Weight:301.265
Hs Code.:

C<sub>14</sub>H<sub>14</sub>F<sub>3</sub>NO<sub>3</sub>

Synonyms:C₁₄H₁₄F₃NO₃

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Chemical Property of C₁₄H₁₄F₃NO₃

Chemical Property:

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Technology Process of C₁₄H₁₄F₃NO₃

There total 3 articles about C₁₄H₁₄F₃NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1234790-83-0
4-(propyloxy)-2-(trifluoromethyl)benzaldehyde oxime

: 107-19-7
propargyl alcohol

: 1234790-98-7
C₁₄H₁₄F₃NO₃

Guidance literature:: 4-(propyloxy)-2-(trifluoromethyl)benzaldehyde oxime; With pyridine; N-chloro-succinimide; In tetrahydrofuran; at 60 ℃; for 0.75h; Inert atmosphere;

propargyl alcohol; With triethylamine; In tetrahydrofuran; at 60 ℃;

Reference yield:

: 1186482-11-0
1-bromo-4-propoxy-2-(trifluoromethyl)benzene

: 1234790-98-7
C₁₄H₁₄F₃NO₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / hexanes; diethyl ether / Cooling with acetone-dry ice; Inert atmosphere

1.2: 20 °C / Cooling with acetone-dry ice

1.3: 0.25 h

2.1: hydroxylamine / ethanol; water / 2 h / 20 °C

3.1: pyridine; N-chloro-succinimide / tetrahydrofuran / 0.75 h / 60 °C / Inert atmosphere

3.2: 60 °C

With pyridine; N-chloro-succinimide; n-butyllithium; hydroxylamine; In tetrahydrofuran; hexanes; diethyl ether; ethanol; water;

Reference yield:

: 40161-55-5
1-bromo-4-fluoro-2-(trifluoromethyl)benzene

: 1234790-98-7
C₁₄H₁₄F₃NO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / mineral oil / 20 - 145 °C / Microwave irradiation; Sealed tube

2.1: n-butyllithium / hexanes; diethyl ether / Cooling with acetone-dry ice; Inert atmosphere

2.2: 20 °C / Cooling with acetone-dry ice

2.3: 0.25 h

3.1: hydroxylamine / ethanol; water / 2 h / 20 °C

4.1: pyridine; N-chloro-succinimide / tetrahydrofuran / 0.75 h / 60 °C / Inert atmosphere

4.2: 60 °C

With pyridine; N-chloro-succinimide; n-butyllithium; hydroxylamine; sodium hydride; In tetrahydrofuran; hexanes; diethyl ether; ethanol; water; mineral oil;