benzhydryl 7β-(phenoxyacetamido)-3β-fluoro-3α-methylcepham 1,1-dioxide

Base Information

Chemical Name:benzhydryl 7β-(phenoxyacetamido)-3β-fluoro-3α-methylcepham 1,1-dioxide
CAS No.:106469-44-7
Molecular Formula:C₂₉H₂₇FN₂O₇S
Molecular Weight:566.607
Hs Code.:

Synonyms:benzhydryl 7β-(phenoxyacetamido)-3β-fluoro-3α-methylcepham 1,1-dioxide

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Chemical Property of benzhydryl 7β-(phenoxyacetamido)-3β-fluoro-3α-methylcepham 1,1-dioxide

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Technology Process of benzhydryl 7β-(phenoxyacetamido)-3β-fluoro-3α-methylcepham 1,1-dioxide

There total 4 articles about benzhydryl 7β-(phenoxyacetamido)-3β-fluoro-3α-methylcepham 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 51415-74-8
benzhydryl 7β-(phenoxyacetamido)-3β-fluoro-3α-methylcepham

: 106469-44-7
benzhydryl 7β-(phenoxyacetamido)-3β-fluoro-3α-methylcepham 1,1-dioxide

Guidance literature:: With potassium permanganate; In water; acetic acid; for 3.5h; Ambient temperature;
DOI:10.1021/jo00381a034

Reference yield:

: 51415-41-9,67977-59-7
(2R,3S,6S)-3-Chloromethyl-3-methyl-7-oxo-6-(2-phenoxy-acetylamino)-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid benzhydryl ester

: 106469-44-7
benzhydryl 7β-(phenoxyacetamido)-3β-fluoro-3α-methylcepham 1,1-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / AgF / CH₂Cl₂ / 48 h / 25 °C

2: 68 percent / KMnO₄ / acetic acid; H₂O / 3.5 h / Ambient temperature

With potassium permanganate; silver fluoride; In dichloromethane; water; acetic acid;
DOI:10.1021/jo00381a034

Reference yield:

: 51415-48-6
benzhydryl 6β-(phenoxyacetamido)-2β-(bromomethyl)penicillinate

: 106469-44-7
benzhydryl 7β-(phenoxyacetamido)-3β-fluoro-3α-methylcepham 1,1-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / AgF / CH₂Cl₂ / 2 h / 25 °C

2: 68 percent / KMnO₄ / acetic acid; H₂O / 3.5 h / Ambient temperature

With potassium permanganate; silver fluoride; In dichloromethane; water; acetic acid;
DOI:10.1021/jo00381a034