Technology Process of N-(4-((diphenylmethylene)amino)phenyl)-N-methylacetamide
There total 2 articles about N-(4-((diphenylmethylene)amino)phenyl)-N-methylacetamide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tris-(dibenzylideneacetone)dipalladium(0); 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate;
In
toluene;
at 80 ℃;
for 12h;
Inert atmosphere;
Schlenk technique;
DOI:10.1021/ja4056239
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.08 h / 0 °C / Inert atmosphere
1.2: 14 h / 20 °C / Inert atmosphere
2.1: tris-(dibenzylideneacetone)dipalladium(0); 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate / toluene / 12 h / 80 °C / Inert atmosphere; Schlenk technique
With
tris-(dibenzylideneacetone)dipalladium(0); sodium hydride; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate;
In
tetrahydrofuran; toluene; mineral oil;
DOI:10.1021/ja4056239
- Guidance literature:
-
With
hydroxylamine hydrochloride; sodium acetate;
In
methanol;
at 20 ℃;
for 1h;
Inert atmosphere;
DOI:10.1021/ja4056239
