methyl (7,8-di-O-benzoyl-4,5-O-isopropylidene-3-deoxy-β-D-manno-2-octulopyranosyl N-phenyl trifluoroacetimidate)onate

Base Information

• Chemical Name: methyl (7,8-di-O-benzoyl-4,5-O-isopropylidene-3-deoxy-β-D-manno-2-octulopyranosyl N-phenyl trifluoroacetimidate)onate
• CAS No.: 1609277-22-6
• Molecular Formula: C₃₄H₃₂F₃NO₁₀
• Molecular Weight: 671.624

Synonyms:methyl (7,8-di-O-benzoyl-4,5-O-isopropylidene-3-deoxy-β-D-manno-2-octulopyranosyl N-phenyl trifluoroacetimidate)onate

Chemical Property of methyl (7,8-di-O-benzoyl-4,5-O-isopropylidene-3-deoxy-β-D-manno-2-octulopyranosyl N-phenyl trifluoroacetimidate)onate

Chemical Property:

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Technology Process of methyl (7,8-di-O-benzoyl-4,5-O-isopropylidene-3-deoxy-β-D-manno-2-octulopyranosyl N-phenyl trifluoroacetimidate)onate

There total 1 articles about methyl (7,8-di-O-benzoyl-4,5-O-isopropylidene-3-deoxy-β-D-manno-2-octulopyranosyl N-phenyl trifluoroacetimidate)onate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl (7,8-di-O-benzoyl-4,5-O-isopropylidene-3-deoxy-D-manno-2-octulopyranoside)onate + 2,2,2-trifluoro-N-phenyl-acetimidoyl chloride (61881-19-4) → methyl (7,8-di-O-benzoyl-4,5-O-isopropylidene-3-deoxy-α-D-manno-2-octulopyranosyl N-phenyl trifluoroacetimidate)onate (1609277-21-5) + methyl (7,8-di-O-benzoyl-4,5-O-isopropylidene-3-deoxy-β-D-manno-2-octulopyranosyl N-phenyl trifluoroacetimidate)onate (1609277-22-6)

Guidance literature:

With potassium carbonate; In dichloromethane; for 168h; Overall yield = 100 %; Overall yield = 343 mg; Inert atmosphere;

DOI:10.1016/j.tet.2014.04.024

Reference yield:

methyl (allyl 7,8-di-O-benzoyl-3-deoxy-α-D-manno-2-octulopyranoside)onate (1327153-97-8) + methyl (7,8-di-O-benzoyl-4,5-O-isopropylidene-3-deoxy-β-D-manno-2-octulopyranosyl N-phenyl trifluoroacetimidate)onate (1609277-22-6) → methyl O-[methyl (7,8-di-O-benzoyl-4,5-O-isopropylidene-3-deoxy-D-manno-2-octulopyranosyl)onate]-(2->4)-(allyl 7,8-di-O-benzoyl-3-deoxy-α-D-manno-2-octulopyranoside)onate (1327154-00-6) + methyl O-[methyl (7,8-di-O-benzoyl-4,5-O-isopropylidene-3-deoxy-D-manno-2-octulopyranosyl)onate]-(2->4)-(allyl 7,8-di-O-benzoyl-3-deoxy-α-D-manno-2-octulopyranoside)onate (1327154-05-1) + C26H26O9 (132039-61-3)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; at -20 - 20 ℃; for 10h;

DOI:10.1016/j.tet.2014.04.024

upstream raw materials:

2,2,2-trifluoro-N-phenyl-acetimidoyl chloride

Downstream raw materials:

methyl O-[methyl (7,8-di-O-benzoyl-4,5-O-isopropylidene-3-deoxy-D-manno-2-octulopyranosyl)onate]-(2->4)-(allyl 7,8-di-O-benzoyl-3-deoxy-α-D-manno-2-octulopyranoside)onate

methyl O-[methyl (7,8-di-O-benzoyl-4,5-O-isopropylidene-3-deoxy-D-manno-2-octulopyranosyl)onate]-(2->4)-(allyl 7,8-di-O-benzoyl-3-deoxy-α-D-manno-2-octulopyranoside)onate

C₂₆H₂₆O₉

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