1,4-dihydro-2-methyl-4-(3-nitrophenyl)-6-<(2-pyrid-3-yl-ethoxy)methyl>pyridine-3,5-dicarboxylic acid 3-methyl 5-ethyl diester

Base Information

Chemical Name:1,4-dihydro-2-methyl-4-(3-nitrophenyl)-6-<(2-pyrid-3-yl-ethoxy)methyl>pyridine-3,5-dicarboxylic acid 3-methyl 5-ethyl diester
CAS No.:123753-96-8
Molecular Formula:C₂₅H₂₇N₃O₇
Molecular Weight:481.505
Hs Code.:

Synonyms:1,4-dihydro-2-methyl-4-(3-nitrophenyl)-6-<(2-pyrid-3-yl-ethoxy)methyl>pyridine-3,5-dicarboxylic acid 3-methyl 5-ethyl diester

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Chemical Property of 1,4-dihydro-2-methyl-4-(3-nitrophenyl)-6-<(2-pyrid-3-yl-ethoxy)methyl>pyridine-3,5-dicarboxylic acid 3-methyl 5-ethyl diester

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Technology Process of 1,4-dihydro-2-methyl-4-(3-nitrophenyl)-6-<(2-pyrid-3-yl-ethoxy)methyl>pyridine-3,5-dicarboxylic acid 3-methyl 5-ethyl diester

There total 4 articles about 1,4-dihydro-2-methyl-4-(3-nitrophenyl)-6-<(2-pyrid-3-yl-ethoxy)methyl>pyridine-3,5-dicarboxylic acid 3-methyl 5-ethyl diester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 119128-13-1
methyl (Z)-2-(3-nitrobenzylidene)-3-oxobutanoate

: 123753-94-6
ethyl 3-oxo-4-(2-pyrid-3-ylethoxy)butanoate

: 123753-96-8
1,4-dihydro-2-methyl-4-(3-nitrophenyl)-6-<(2-pyrid-3-yl-ethoxy)methyl>pyridine-3,5-dicarboxylic acid 3-methyl 5-ethyl diester

: 123754-06-3
1,4-dihydro-4-(3-nitrophenyl)-2,6-bis<(2-pyrid-3-ylethoxy)methyl>pyridine-3,5-dicarboxylic acid diethyl ester

Guidance literature:: With ammonium hydroxide; In ethanol; for 6h; Heating;
DOI:10.1021/jm00164a028

Reference yield:

: methyl 3-nitrobenzylidienacetoacetate

: 123753-94-6
ethyl 3-oxo-4-(2-pyrid-3-ylethoxy)butanoate

: 123753-96-8
1,4-dihydro-2-methyl-4-(3-nitrophenyl)-6-<(2-pyrid-3-yl-ethoxy)methyl>pyridine-3,5-dicarboxylic acid 3-methyl 5-ethyl diester

Guidance literature:: With hydrogenchloride; conc. ammonia; In ethanol; ethyl acetate;

Reference yield:

: 6293-56-7
3-pyridinylethanol

: 123753-96-8
1,4-dihydro-2-methyl-4-(3-nitrophenyl)-6-<(2-pyrid-3-yl-ethoxy)methyl>pyridine-3,5-dicarboxylic acid 3-methyl 5-ethyl diester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium hydride / 1.) THF, mineral oil, 2.) THF, overnight

2: 2.7 g / concd aq. NH₃ / ethanol / 6 h / Heating

With ammonium hydroxide; sodium hydride; In ethanol;
DOI:10.1021/jm00164a028