N,N'-bis(tert-butoxycarbonyl)-N,N'-bis(4-hydroxymethylbenzyl)-1,6-hexanediamine

Base Information

Chemical Name:N,N'-bis(tert-butoxycarbonyl)-N,N'-bis(4-hydroxymethylbenzyl)-1,6-hexanediamine
CAS No.:264191-34-6
Molecular Formula:C₃₂H₄₈N₂O₆
Molecular Weight:556.743
Hs Code.:

Synonyms:N,N'-bis(tert-butoxycarbonyl)-N,N'-bis(4-hydroxymethylbenzyl)-1,6-hexanediamine

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Chemical Property of N,N'-bis(tert-butoxycarbonyl)-N,N'-bis(4-hydroxymethylbenzyl)-1,6-hexanediamine

Chemical Property:

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Technology Process of N,N'-bis(tert-butoxycarbonyl)-N,N'-bis(4-hydroxymethylbenzyl)-1,6-hexanediamine

There total 6 articles about N,N'-bis(tert-butoxycarbonyl)-N,N'-bis(4-hydroxymethylbenzyl)-1,6-hexanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 264191-33-5
N,N'-bis(tert-butoxycarbonyl)-N,N'-bis(4-methoxycarbonylbenzyl)-1,6-hexanediamine

: 264191-34-6
N,N'-bis(tert-butoxycarbonyl)-N,N'-bis(4-hydroxymethylbenzyl)-1,6-hexanediamine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 0.5h; Heating;
DOI:10.1021/jo991397w

Reference yield:

: 264191-32-4
N,N'-bis(4-methoxycarbonylbenzyl)-1,6-hexanediamine

: 264191-34-6
N,N'-bis(tert-butoxycarbonyl)-N,N'-bis(4-hydroxymethylbenzyl)-1,6-hexanediamine

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / DMAP / CH₂Cl₂ / 3 h / 20 °C

2: 86 percent / LiAlH₄ / tetrahydrofuran / 0.5 h / Heating

With dmap; lithium aluminium tetrahydride; In tetrahydrofuran; dichloromethane; 1: Acylation / 2: Reduction;
DOI:10.1021/jo991397w

Reference yield:

: 124-09-4
1,6-Hexanediamine

: 264191-34-6
N,N'-bis(tert-butoxycarbonyl)-N,N'-bis(4-hydroxymethylbenzyl)-1,6-hexanediamine

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / toluene / 0.5 h / Heating

2: 93 percent / NaBH₄ / methanol / 1 h / Heating

3: 100 percent / DMAP / CH₂Cl₂ / 3 h / 20 °C

4: 86 percent / LiAlH₄ / tetrahydrofuran / 0.5 h / Heating

With dmap; sodium tetrahydroborate; lithium aluminium tetrahydride; In tetrahydrofuran; methanol; dichloromethane; toluene; 1: Condensation / 2: Reduction / 3: Acylation / 4: Reduction;
DOI:10.1021/jo991397w