Technology Process of cis-N-nitroso-2,4-diphenylazetidine
There total 10 articles about cis-N-nitroso-2,4-diphenylazetidine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium nitrite;
In
water; acetic acid;
1. 0.5h, 0 degC; 2. r.t., 33h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: lithium aluminum hydride / diethyl ether / 6 h / Heating
2: 7.03 g / HCl (g), thionyl chloride / tetrahydrofuran / 0.5 h / Ambient temperature
3: 98 percent / pyridine / 2 h
4: sodium ethoxide / ethanol / 1.5 h
5: 11 percent / sodium / pentan-1-ol / Ambient temperature; overnight
6: 1. methyl lithium; 2. nitrosyl chloride / 1. ether, 5 min; 2. dimethoxyethane, 5 min
With
hydrogenchloride; lithium aluminium tetrahydride; thionyl chloride; methyllithium; sodium ethanolate; sodium; nitrosylchloride;
In
tetrahydrofuran; pyridine; diethyl ether; ethanol; pentan-1-ol;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 7.03 g / HCl (g), thionyl chloride / tetrahydrofuran / 0.5 h / Ambient temperature
2: 98 percent / pyridine / 2 h
3: sodium ethoxide / ethanol / 1.5 h
4: 11 percent / sodium / pentan-1-ol / Ambient temperature; overnight
5: 1. methyl lithium; 2. nitrosyl chloride / 1. ether, 5 min; 2. dimethoxyethane, 5 min
With
hydrogenchloride; thionyl chloride; methyllithium; sodium ethanolate; sodium; nitrosylchloride;
In
tetrahydrofuran; pyridine; ethanol; pentan-1-ol;
