C₁₈H₁₄O₈*C₂₇H₃₄ClN₅O₃

Base Information

Chemical Name:C₁₈H₁₄O₈*C₂₇H₃₄ClN₅O₃
CAS No.:1372127-17-7
Molecular Formula:C₁₈H₁₄O₈*C₂₇H₃₄ClN₅O₃
Molecular Weight:870.356
Hs Code.:

C<sub>18</sub>H<sub>14</sub>O<sub>8</sub>*C<sub>27</sub>H<sub>34</sub>ClN<sub>5</sub>O<sub>3</sub>

Synonyms:C₁₈H₁₄O₈*C₂₇H₃₄ClN₅O₃

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Chemical Property of C₁₈H₁₄O₈*C₂₇H₃₄ClN₅O₃

Chemical Property:

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Technology Process of C₁₈H₁₄O₈*C₂₇H₃₄ClN₅O₃

There total 15 articles about C₁₈H₁₄O₈*C₂₇H₃₄ClN₅O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1251528-23-0
C₂₇H₃₄ClN₅O₃

: 17026-42-5
O,O'-dibenzoyl-D-tartaric acid

: 1372127-17-7
C₁₈H₁₄O₈*C₂₇H₃₄ClN₅O₃

Guidance literature:: C₂₇H₃₄ClN₅O₃; O,O'-dibenzoyl-D-tartaric acid; In ethanol; water; at 70 ℃;

In ethanol; water;

Reference yield:

: 25462-85-5
2-chloro-6-methylpyridine-4-carboxylic acid

: 1372127-17-7
C₁₈H₁₄O₈*C₂₇H₃₄ClN₅O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: thionyl chloride / N,N-dimethyl-formamide; toluene / 1.5 h / Reflux

1.2: 1.5 h / 20 °C

2.1: caesium carbonate; benzophenoneimine / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 48 h / 100 °C

3.1: triethylamine / tetrahydrofuran / 55 °C

3.2: 1 h

4.1: ethanol; water / 70 °C

With thionyl chloride; benzophenoneimine; caesium carbonate; triethylamine; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1251530-05-8
2-Chloro-6,N,N-trimethyl-isonicotinamide

: 1372127-17-7
C₁₈H₁₄O₈*C₂₇H₃₄ClN₅O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: caesium carbonate; benzophenoneimine / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 48 h / 100 °C

2.1: triethylamine / tetrahydrofuran / 55 °C

2.2: 1 h

3.1: ethanol; water / 70 °C

With benzophenoneimine; caesium carbonate; triethylamine; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In tetrahydrofuran; ethanol; water; toluene;