C₃₂H₄₁NO₄Si

Base Information

Chemical Name:C₃₂H₄₁NO₄Si
CAS No.:1431116-76-5
Molecular Formula:C₃₂H₄₁NO₄Si
Molecular Weight:531.767
Hs Code.:

C<sub>32</sub>H<sub>41</sub>NO<sub>4</sub>Si

Synonyms:C₃₂H₄₁NO₄Si

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Chemical Property of C₃₂H₄₁NO₄Si

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Technology Process of C₃₂H₄₁NO₄Si

There total 23 articles about C₃₂H₄₁NO₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1431116-74-3
C₁₆H₂₃NO₄

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1431116-76-5
C₃₂H₄₁NO₄Si

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1016/j.tet.2013.03.012

Reference yield:

: C₂₃H₃₁NO₇S

: 1431116-76-5
C₃₂H₄₁NO₄Si

Guidance literature:: Multi-step reaction with 20 steps

1.1: 1H-imidazole / tetrahydrofuran / 24 h / 0 - 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 0 - 20 °C

3.1: potassium iodide; sodium hydride / tetrahydrofuran / 6 h / 60 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C

5.1: Dess-Martin periodane / dichloromethane / 1 h / 0 °C / Inert atmosphere

6.1: dichloromethane / 2 h / 20 °C / Inert atmosphere

7.1: diisobutylaluminium hydride / dichloromethane; toluene / 1 h / 78 °C / Inert atmosphere

8.1: titanium(IV) isopropylate; L-(+)-diisopropyl tartrate / dichloromethane / 0.5 h / -30 °C / Inert atmosphere

8.2: 15 h / -30 °C / Inert atmosphere

9.1: Dess-Martin periodane / dichloromethane / 1 h / 0 °C / Inert atmosphere

10.1: dichloromethane / 2 h / 20 °C / Inert atmosphere

11.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 7 h / -30 - 20 °C / Inert atmosphere

12.1: ozone / methanol; dichloromethane / 2 h / -70 °C

13.1: sodium tetrahydroborate / methanol; dichloromethane / 23 h

14.1: triethylamine; dmap / dichloromethane / 14 h / 20 °C

15.1: sodium hydride / tetrahydrofuran / 17 h / 0 - 20 °C

16.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

17.1: naphthalene; sodium / 1,2-dimethoxyethane / -70 °C / Inert atmosphere

18.1: 1H-imidazole; triphenylphosphine; iodine / acetonitrile; diethyl ether / 18 h / 20 °C

19.1: palladium on carbon; hydrogen; hydrogenchloride / methanol / 2 h / 0 - 20 °C

20.1: triethylamine; dmap / dichloromethane / 1 h / 20 °C

With 1H-imidazole; titanium(IV) isopropylate; hydrogenchloride; dmap; sodium tetrahydroborate; lithium aluminium tetrahydride; naphthalene; L-(+)-diisopropyl tartrate; trimethylsilyl trifluoromethanesulfonate; palladium on carbon; tetrabutyl ammonium fluoride; hydrogen; iodine; sodium; sodium hydride; diisobutylaluminium hydride; Dess-Martin periodane; ozone; triethylamine; triphenylphosphine; potassium iodide; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; diethyl ether; dichloromethane; toluene; acetonitrile; 5.1: |Dess-Martin Oxidation / 6.1: |Wittig Olefination / 9.1: |Dess-Martin Oxidation / 10.1: |Wittig Olefination;
DOI:10.1016/j.tet.2013.03.012

Reference yield:

: C₃₉H₄₉NO₇SSi

: 1431116-76-5
C₃₂H₄₁NO₄Si

Guidance literature:: Multi-step reaction with 19 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 0 - 20 °C

2.1: potassium iodide; sodium hydride / tetrahydrofuran / 6 h / 60 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C

4.1: Dess-Martin periodane / dichloromethane / 1 h / 0 °C / Inert atmosphere

5.1: dichloromethane / 2 h / 20 °C / Inert atmosphere

6.1: diisobutylaluminium hydride / dichloromethane; toluene / 1 h / 78 °C / Inert atmosphere

7.1: titanium(IV) isopropylate; L-(+)-diisopropyl tartrate / dichloromethane / 0.5 h / -30 °C / Inert atmosphere

7.2: 15 h / -30 °C / Inert atmosphere

8.1: Dess-Martin periodane / dichloromethane / 1 h / 0 °C / Inert atmosphere

9.1: dichloromethane / 2 h / 20 °C / Inert atmosphere

10.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 7 h / -30 - 20 °C / Inert atmosphere

11.1: ozone / methanol; dichloromethane / 2 h / -70 °C

12.1: sodium tetrahydroborate / methanol; dichloromethane / 23 h

13.1: triethylamine; dmap / dichloromethane / 14 h / 20 °C

14.1: sodium hydride / tetrahydrofuran / 17 h / 0 - 20 °C

15.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

16.1: naphthalene; sodium / 1,2-dimethoxyethane / -70 °C / Inert atmosphere

17.1: 1H-imidazole; triphenylphosphine; iodine / acetonitrile; diethyl ether / 18 h / 20 °C

18.1: palladium on carbon; hydrogen; hydrogenchloride / methanol / 2 h / 0 - 20 °C

19.1: triethylamine; dmap / dichloromethane / 1 h / 20 °C

With 1H-imidazole; titanium(IV) isopropylate; hydrogenchloride; dmap; sodium tetrahydroborate; lithium aluminium tetrahydride; naphthalene; L-(+)-diisopropyl tartrate; trimethylsilyl trifluoromethanesulfonate; palladium on carbon; tetrabutyl ammonium fluoride; hydrogen; iodine; sodium; sodium hydride; diisobutylaluminium hydride; Dess-Martin periodane; ozone; triethylamine; triphenylphosphine; potassium iodide; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; diethyl ether; dichloromethane; toluene; acetonitrile; 4.1: |Dess-Martin Oxidation / 5.1: |Wittig Olefination / 8.1: |Dess-Martin Oxidation / 9.1: |Wittig Olefination;
DOI:10.1016/j.tet.2013.03.012