phenylmethyl (2E)-3-(4-{[4-(4-{[3-(3,3-dimethyl-1-piperidinyl)propyl]oxy}phenyl)-1-piperidinyl]-carbonyl}-1-naphthalenyl)-2-propenoate fumarate

Base Information

Chemical Name:phenylmethyl (2E)-3-(4-{[4-(4-{[3-(3,3-dimethyl-1-piperidinyl)propyl]oxy}phenyl)-1-piperidinyl]-carbonyl}-1-naphthalenyl)-2-propenoate fumarate
CAS No.:1256920-60-1
Molecular Formula:C₄H₄O₄*C₄₂H₄₈N₂O₄
Molecular Weight:760.927
Hs Code.:

Synonyms:phenylmethyl (2E)-3-(4-{[4-(4-{[3-(3,3-dimethyl-1-piperidinyl)propyl]oxy}phenyl)-1-piperidinyl]-carbonyl}-1-naphthalenyl)-2-propenoate fumarate

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Chemical Property of phenylmethyl (2E)-3-(4-{[4-(4-{[3-(3,3-dimethyl-1-piperidinyl)propyl]oxy}phenyl)-1-piperidinyl]-carbonyl}-1-naphthalenyl)-2-propenoate fumarate

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Technology Process of phenylmethyl (2E)-3-(4-{[4-(4-{[3-(3,3-dimethyl-1-piperidinyl)propyl]oxy}phenyl)-1-piperidinyl]-carbonyl}-1-naphthalenyl)-2-propenoate fumarate

There total 6 articles about phenylmethyl (2E)-3-(4-{[4-(4-{[3-(3,3-dimethyl-1-piperidinyl)propyl]oxy}phenyl)-1-piperidinyl]-carbonyl}-1-naphthalenyl)-2-propenoate fumarate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 942260-20-0
4-{(1E)-3-oxo-3-[(phenylmethyl)oxy]-1-propen-1-yl}-1-naphthalenecarboxylic acid

: 1256920-60-1
phenylmethyl (2E)-3-(4-{[4-(4-{[3-(3,3-dimethyl-1-piperidinyl)propyl]oxy}phenyl)-1-piperidinyl]-carbonyl}-1-naphthalenyl)-2-propenoate fumarate

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / Isopropyl acetate / 79 °C

2: potassium carbonate / Isopropyl acetate; water / 55 °C

3: isopropyl alcohol / 70 °C / Large scale reaction

With thionyl chloride; potassium carbonate; In Isopropyl acetate; water; isopropyl alcohol;
DOI:10.1021/op1002598

Reference yield:

: 942347-52-6
C₂₁H₃₄N₂O

: 1256920-60-1
phenylmethyl (2E)-3-(4-{[4-(4-{[3-(3,3-dimethyl-1-piperidinyl)propyl]oxy}phenyl)-1-piperidinyl]-carbonyl}-1-naphthalenyl)-2-propenoate fumarate

Guidance literature:: Multi-step reaction with 3 steps

1: 1 h / 20 °C / Large scale reaction

2: potassium carbonate / Isopropyl acetate; water / 55 °C

3: isopropyl alcohol / 70 °C / Large scale reaction

With potassium carbonate; In Isopropyl acetate; water; isopropyl alcohol;
DOI:10.1021/op1002598

Reference yield:

: C₂₁H₁₅ClO₃

: 1256920-60-1
phenylmethyl (2E)-3-(4-{[4-(4-{[3-(3,3-dimethyl-1-piperidinyl)propyl]oxy}phenyl)-1-piperidinyl]-carbonyl}-1-naphthalenyl)-2-propenoate fumarate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / Isopropyl acetate; water / 55 °C

2: isopropyl alcohol / 70 °C / Large scale reaction

With potassium carbonate; In Isopropyl acetate; water; isopropyl alcohol;
DOI:10.1021/op1002598