1-(4-[4-((2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl)carbonyl-2-methoxy-5-nitrophenoxy]butyl)-1,2-dihydrobenzo[c,d]indol-2-one

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Chemical Name:1-(4-[4-((2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl)carbonyl-2-methoxy-5-nitrophenoxy]butyl)-1,2-dihydrobenzo[c,d]indol-2-one
CAS No.:1357113-96-2
Molecular Formula:C₃₂H₃₇N₃O₆S₂
Molecular Weight:623.794
Hs Code.:

Synonyms:1-(4-[4-((2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl)carbonyl-2-methoxy-5-nitrophenoxy]butyl)-1,2-dihydrobenzo[c,d]indol-2-one

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Chemical Property of 1-(4-[4-((2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl)carbonyl-2-methoxy-5-nitrophenoxy]butyl)-1,2-dihydrobenzo[c,d]indol-2-one

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Technology Process of 1-(4-[4-((2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl)carbonyl-2-methoxy-5-nitrophenoxy]butyl)-1,2-dihydrobenzo[c,d]indol-2-one

There total 4 articles about 1-(4-[4-((2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl)carbonyl-2-methoxy-5-nitrophenoxy]butyl)-1,2-dihydrobenzo[c,d]indol-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 130-00-7
1,8-naphtholactam

: 343308-56-5
(2S)-N-[4-(4-bromobutyl)oxy-5-methoxy-2-nitrobenzoyl]pyrrolidine-2-carboxaldehyde diethylthioacetal

: 1357113-96-2
1-(4-[4-((2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl)carbonyl-2-methoxy-5-nitrophenoxy]butyl)-1,2-dihydrobenzo[c,d]indol-2-one

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.bmc.2011.12.003

Reference yield:

: 7797-81-1
N-hydroxy-1,8-naphthalenedicarboximide

: 1357113-96-2
1-(4-[4-((2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl)carbonyl-2-methoxy-5-nitrophenoxy]butyl)-1,2-dihydrobenzo[c,d]indol-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: p-toluenesulfonyl chloride / 1 h / Heating

2: sodium hydride / N,N-dimethyl-formamide / 20 °C

With sodium hydride; p-toluenesulfonyl chloride; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.12.003

Reference yield:

: 81-84-5
1,8-Naphthalic anhydride

: 1357113-96-2
1-(4-[4-((2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl)carbonyl-2-methoxy-5-nitrophenoxy]butyl)-1,2-dihydrobenzo[c,d]indol-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; hydroxylamine hydrochloride / 1 h / Reflux

2: p-toluenesulfonyl chloride / 1 h / Heating

3: sodium hydride / N,N-dimethyl-formamide / 20 °C

With pyridine; hydroxylamine hydrochloride; sodium hydride; p-toluenesulfonyl chloride; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.12.003