(Z)-3-(mesitylsulfonyl)-5-phenyl-3,7,8,9-tetrahydro-2H-1,6,3-dioxazonine

Base Information

Chemical Name:(Z)-3-(mesitylsulfonyl)-5-phenyl-3,7,8,9-tetrahydro-2H-1,6,3-dioxazonine
CAS No.:1612143-23-3
Molecular Formula:C₂₁H₂₅NO₄S
Molecular Weight:387.5
Hs Code.:

Synonyms:(Z)-3-(mesitylsulfonyl)-5-phenyl-3,7,8,9-tetrahydro-2H-1,6,3-dioxazonine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-3-(mesitylsulfonyl)-5-phenyl-3,7,8,9-tetrahydro-2H-1,6,3-dioxazonine

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Technology Process of (Z)-3-(mesitylsulfonyl)-5-phenyl-3,7,8,9-tetrahydro-2H-1,6,3-dioxazonine

There total 3 articles about (Z)-3-(mesitylsulfonyl)-5-phenyl-3,7,8,9-tetrahydro-2H-1,6,3-dioxazonine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 505-22-6
1,3-dioxane

: 1612143-05-1
1-(mesitylsulfonyl)-4-phenyl-1H-1,2,3-triazole

: 1612143-23-3
(Z)-3-(mesitylsulfonyl)-5-phenyl-3,7,8,9-tetrahydro-2H-1,6,3-dioxazonine

Guidance literature:: With dirhodium tetraacetate; at 100 ℃; for 5h; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol5012532

Reference yield:

: 773-64-8
2-mesitylenesulphonyl chloride

: 1612143-23-3
(Z)-3-(mesitylsulfonyl)-5-phenyl-3,7,8,9-tetrahydro-2H-1,6,3-dioxazonine

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / acetone; water / 0 - 20 °C

2: copper(I) thiophene-2-carboxylate / water; toluene / 20 °C / Darkness

3: dirhodium tetraacetate / 5 h / 100 °C / Inert atmosphere

With dirhodium tetraacetate; sodium azide; copper(I) thiophene-2-carboxylate; In water; acetone; toluene; 2: |Huisgen Cycloaddition;
DOI:10.1021/ol5012532

Reference yield:

: 24906-63-6
2,4,6-trimethylbenzene-1-sulfonyl azide

: 1612143-23-3
(Z)-3-(mesitylsulfonyl)-5-phenyl-3,7,8,9-tetrahydro-2H-1,6,3-dioxazonine

Guidance literature:: Multi-step reaction with 2 steps

1: copper(I) thiophene-2-carboxylate / water; toluene / 20 °C / Darkness

2: dirhodium tetraacetate / 5 h / 100 °C / Inert atmosphere

With dirhodium tetraacetate; copper(I) thiophene-2-carboxylate; In water; toluene; 1: |Huisgen Cycloaddition;
DOI:10.1021/ol5012532