5-phenyl-5,6-dihydrophenanthridine

Base Information

Chemical Name:5-phenyl-5,6-dihydrophenanthridine
CAS No.:13355-64-1
Molecular Formula:C₁₉H₁₅N
Molecular Weight:257.335
Hs Code.:

Synonyms:5-phenyl-5,6-dihydrophenanthridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-phenyl-5,6-dihydrophenanthridine

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Technology Process of 5-phenyl-5,6-dihydrophenanthridine

There total 8 articles about 5-phenyl-5,6-dihydrophenanthridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: (2-bromobenzyl)diphenylamine

: 13355-64-1
5-phenyl-5,6-dihydrophenanthridine

Guidance literature:: With palladium diacetate; trimethylbenzylammonium bromide; potassium carbonate; In N,N-dimethyl-formamide; at 120 ℃; for 9h; Inert atmosphere;

Reference yield: 73.0%

: N-((2'-methoxy-[1,1'-biphenyl]-2-yl)methyl)aniline

: 13355-64-1
5-phenyl-5,6-dihydrophenanthridine

Guidance literature:: With phosphazene base-P₄-tert-butyl; In 1,4-dioxane; hexane; at 120 ℃; for 18h; Inert atmosphere; Molecular sieve; Sealed tube;
DOI:10.1021/acs.orglett.9b01805

Reference yield:

: C₂₀H₁₇NO

: 13355-64-1
5-phenyl-5,6-dihydrophenanthridine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / tetrahydrofuran; methanol / 5 h / 0 - 20 °C / Inert atmosphere

2: phosphazene base-P₄-tert-butyl / hexane; 1,4-dioxane / 18 h / 120 °C / Inert atmosphere; Molecular sieve; Sealed tube

With sodium tetrahydroborate; phosphazene base-P₄-tert-butyl; In tetrahydrofuran; 1,4-dioxane; methanol; hexane;
DOI:10.1021/acs.orglett.9b01805