benzyl 7-chlorocarbonyl-2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoate

Base Information

Chemical Name:benzyl 7-chlorocarbonyl-2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoate
CAS No.:1355356-58-9
Molecular Formula:C₁₅H₇ClF₁₂O₃
Molecular Weight:498.653
Hs Code.:

Synonyms:benzyl 7-chlorocarbonyl-2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 7-chlorocarbonyl-2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoate

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Technology Process of benzyl 7-chlorocarbonyl-2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoate

There total 3 articles about benzyl 7-chlorocarbonyl-2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1967-93-7
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioyl dichloride

: 100-51-6,185532-71-2
benzyl alcohol

: 1355356-58-9
benzyl 7-chlorocarbonyl-2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoate

Guidance literature:: at 100 ℃; for 2h; Inert atmosphere; Cooling with ice;
DOI:10.1016/j.bmc.2011.11.041

Reference yield:

: 678-45-5
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid

: 1355356-58-9
benzyl 7-chlorocarbonyl-2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoate

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride; N,N-dimethyl-formamide / 4 h / Inert atmosphere; Reflux

2: 2 h / 100 °C / Inert atmosphere; Cooling with ice

With thionyl chloride; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.11.041

Reference yield:

: 678-45-5
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid

: 100-51-6,185532-71-2
benzyl alcohol

: 1355356-58-9
benzyl 7-chlorocarbonyl-2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoate

Guidance literature:: 2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid; With thionyl chloride; In N,N-dimethyl-formamide;

benzyl alcohol;
DOI:10.1016/j.bmcl.2017.02.050