N-(4-bromobenzyl)-1-((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)-N-methylmethanamine hydrochloride

Base Information

Chemical Name:N-(4-bromobenzyl)-1-((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)-N-methylmethanamine hydrochloride
CAS No.:1313884-68-2
Molecular Formula:C₁₈H₂₄BrN*ClH
Molecular Weight:370.76
Hs Code.:

Synonyms:N-(4-bromobenzyl)-1-((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)-N-methylmethanamine hydrochloride

Suppliers and Price of N-(4-bromobenzyl)-1-((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)-N-methylmethanamine hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-(4-bromobenzyl)-1-((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)-N-methylmethanamine hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-(4-bromobenzyl)-1-((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)-N-methylmethanamine hydrochloride

There total 3 articles about N-(4-bromobenzyl)-1-((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)-N-methylmethanamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 348633-10-3
1-((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)-N-methylmethanamine

: 1122-91-4
4-bromo-benzaldehyde

: 1313884-68-2
N-(4-bromobenzyl)-1-((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)-N-methylmethanamine hydrochloride

Guidance literature:: 1-((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)-N-methylmethanamine; 4-bromo-benzaldehyde; With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 20 ℃; for 20h;

With hydrogenchloride; In diethyl ether;
DOI:10.1016/j.bmc.2011.04.035

Reference yield:

: C₁₁H₁₇N

: 1313884-68-2
N-(4-bromobenzyl)-1-((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)-N-methylmethanamine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol; ethanol / 3 h / 20 °C / Cooling with ice

2: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 h / 20 °C

With sodium tetrahydroborate; sodium tris(acetoxy)borohydride; In methanol; ethanol; 1,2-dichloro-ethane;
DOI:10.1016/j.bmc.2011.04.035

Reference yield:

: 564-94-3,18486-69-6
myrtenal

: 1313884-68-2
N-(4-bromobenzyl)-1-((1R,5S)-6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)-N-methylmethanamine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: methanol; ethanol / 20 °C

2: sodium tetrahydroborate / methanol; ethanol / 3 h / 20 °C / Cooling with ice

3: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 h / 20 °C

With sodium tetrahydroborate; sodium tris(acetoxy)borohydride; In methanol; ethanol; 1,2-dichloro-ethane;
DOI:10.1016/j.bmc.2011.04.035