Carbamic acid, [(1R,4R)-4-hydroxy-1-methyl-2-pentenyl]-, 1,1-dimethylethyl

Base Information

Chemical Name:Carbamic acid, [(1R,4R)-4-hydroxy-1-methyl-2-pentenyl]-, 1,1-dimethylethyl
CAS No.:740798-72-5
Molecular Formula:C₁₁H₂₁NO₃
Molecular Weight:215.293
Hs Code.:
Mol file:740798-72-5.mol

Synonyms:Carbamic acid, [(1R,4R)-4-hydroxy-1-methyl-2-pentenyl]-, 1,1-dimethylethyl

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Chemical Property of Carbamic acid, [(1R,4R)-4-hydroxy-1-methyl-2-pentenyl]-, 1,1-dimethylethyl

Chemical Property:

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Technology Process of Carbamic acid, [(1R,4R)-4-hydroxy-1-methyl-2-pentenyl]-, 1,1-dimethylethyl

There total 5 articles about Carbamic acid, [(1R,4R)-4-hydroxy-1-methyl-2-pentenyl]-, 1,1-dimethylethyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 3,6-dimethyl-3,6-dihydro-[1,2]oxazine-2-carboxylic acid tert-butyl ester

: 740798-72-5
t-butyl (+/-)-(1R,4S)-(4-hydroxy-1-methylpent-2-enyl)carbamate

Guidance literature:: 3,6-dimethyl-3,6-dihydro-[1,2]oxazine-2-carboxylic acid tert-butyl ester; With hexacarbonyl molybdenum; In water; acetonitrile; at 20 ℃; for 0.166667h;

With sodium tetrahydroborate; In water; acetonitrile; at 90 ℃;
DOI:10.1055/s-2005-918457

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 5194-51-4
(2E)-2,6-hexadiene

: 740798-68-9
acetic acid 2,2-dimethyl-5-nitroso-[1,3]dioxan-5-yl ester

: 740798-72-5
t-butyl (+/-)-(1R,4S)-(4-hydroxy-1-methylpent-2-enyl)carbamate

: 740798-72-5
t-butyl (+/-)-(1S,4S)-(4-hydroxy-1-methylpent-2-enyl)carbamate

Guidance literature:: (2E)-2,6-hexadiene; acetic acid 2,2-dimethyl-5-nitroso-[1,3]dioxan-5-yl ester; With copper(II) bis(trifluoromethanesulfonate); In toluene; at 0 ℃;

With hydrogenchloride; In toluene; at 20 ℃; for 0.75h;

di-tert-butyl dicarbonate; With sodium hydroxide; In acetone; toluene; at 20 ℃; pH=10;
DOI:10.1021/ol0491336

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 5194-51-4
(2E)-2,6-hexadiene

: 740798-68-9
acetic acid 2,2-dimethyl-5-nitroso-[1,3]dioxan-5-yl ester

: 740798-72-5
t-butyl (+/-)-(1R,4S)-(4-hydroxy-1-methylpent-2-enyl)carbamate

: 740798-72-5
t-butyl (+/-)-(1S,4S)-(4-hydroxy-1-methylpent-2-enyl)carbamate

Guidance literature:: (2E)-2,6-hexadiene; acetic acid 2,2-dimethyl-5-nitroso-[1,3]dioxan-5-yl ester; With copper(II) bis(trifluoromethanesulfonate); In toluene; at 0 ℃;

With hydrogenchloride; In toluene; at 20 ℃; for 0.75h;

di-tert-butyl dicarbonate; With sodium hydroxide; In acetone; toluene; at 20 ℃; pH=10;
DOI:10.1021/ol0491336