3-phenoxysulfonyl-1-propanesulfonic acid 4-(N-CBz-L-valinamido)-2,2-dimethyl-1-butyl ester

Base Information

Chemical Name:3-phenoxysulfonyl-1-propanesulfonic acid 4-(N-CBz-L-valinamido)-2,2-dimethyl-1-butyl ester
CAS No.:1266342-62-4
Molecular Formula:C₂₈H₄₀N₂O₉S₂
Molecular Weight:612.766
Hs Code.:

Synonyms:3-phenoxysulfonyl-1-propanesulfonic acid 4-(N-CBz-L-valinamido)-2,2-dimethyl-1-butyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-phenoxysulfonyl-1-propanesulfonic acid 4-(N-CBz-L-valinamido)-2,2-dimethyl-1-butyl ester

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Technology Process of 3-phenoxysulfonyl-1-propanesulfonic acid 4-(N-CBz-L-valinamido)-2,2-dimethyl-1-butyl ester

There total 4 articles about 3-phenoxysulfonyl-1-propanesulfonic acid 4-(N-CBz-L-valinamido)-2,2-dimethyl-1-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1266342-27-1
3-phenoxysulfonyl-1-propanesulfonyl chloride

: 1266342-60-2
4-(N-CBz-L-valinamido)-2,2-dimethyl-1-butanol

: 1266342-62-4
3-phenoxysulfonyl-1-propanesulfonic acid 4-(N-CBz-L-valinamido)-2,2-dimethyl-1-butyl ester

Guidance literature:: With pyridine;

Reference yield:

: 103804-80-4
3,3-dimethyl-4-hydroxy butyronitrile

: 1266342-62-4
3-phenoxysulfonyl-1-propanesulfonic acid 4-(N-CBz-L-valinamido)-2,2-dimethyl-1-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen; ammonium hydroxide / Raney nickel / ethanol; water / 48 h / 760.05 Torr

2: sodium hydrogencarbonate / water; tetrahydrofuran / 18 h

3: pyridine

With pyridine; ammonium hydroxide; hydrogen; sodium hydrogencarbonate; Raney nickel; In tetrahydrofuran; ethanol; water;

Reference yield:

: 40894-00-6
3-bromo-2,2-dimethyl-propan-1-ol

: 1266342-62-4
3-phenoxysulfonyl-1-propanesulfonic acid 4-(N-CBz-L-valinamido)-2,2-dimethyl-1-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: dimethyl sulfoxide / 100 °C

2: hydrogen; ammonium hydroxide / Raney nickel / ethanol; water / 48 h / 760.05 Torr

3: sodium hydrogencarbonate / water; tetrahydrofuran / 18 h

4: pyridine

With pyridine; ammonium hydroxide; hydrogen; sodium hydrogencarbonate; Raney nickel; In tetrahydrofuran; ethanol; water; dimethyl sulfoxide;